Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2016, Issue 1, Pages 31-35Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201501223
Keywords
Mechanochemistry; Nitrogen heterocycles; Amines; Heterogeneous catalysis; Ball milling
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Funding
- French government through PHC GILIBERT [28470XG]
- Lithuanian government through PHC GILIBERT [28470XG]
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A straightforward and solventless synthesis of pyrroles was developed by using mechanochemical activation and a biosourced organic acid as the catalyst. Relative to traditional Paal-Knorr methodologies, various N-substituted pyrroles were obtained in very short reaction times. By reaction with unreactive diketones, desymmetrized aliphatic and aromatic compounds were also synthesized.
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