Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2015, Issue 11, Pages 2351-2355Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201500227
Keywords
Bismuth; Green chemistry; Solvent-free reactions; Cyclization; Heterocycles
Categories
Funding
- Ministry of Education ARC [R-143-000-476-112, R-143-000-550-112]
- National University of Singapore (NUS)
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An extensive array of 4H-pyrido[1,2-a]pyrimidin-4-ones have been synthesized from commercially available 2-aminopyridines and -oxo esters with excellent yields under solvent-free conditions. The reaction, catalyzed by cheap and nontoxic BiCl3, proceeds with short reaction times under mild conditions and normal atmosphere. Only water and alcohol are formed as co-products in this green reaction.
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