Journal
NANOSCIENCE AND NANOTECHNOLOGY LETTERS
Volume 9, Issue 1, Pages 56-60Publisher
AMER SCIENTIFIC PUBLISHERS
DOI: 10.1166/nnl.2017.2267
Keywords
Microstructure; Powder Technology; Nanoparticles; Hydrothermal Reaction; Hollow Tubular Structure; MoS2
Funding
- Guangzhou Science and Technology Plan Project [201541]
- Innovation and Strengthen University Project of Guangzhou Maritime University [A330106, B510647]
- Xinjiang Bureau of Quality and Technical Supervision [2013-01]
- science and technology project of State Quality Inspection Administration [2013QK-086]
- Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry [49]
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Molybdenum disulfide (MoS2) with a hollow tubular morphology was successfully prepared via hydrothermal reaction at 200 degrees C using the single-source precursor Mo((C2H5)NCS2)(2)O-2 as both the molybdenum and sulfur sources, sodium silicate (Na2SiO3 center dot 9H(2)O) as the template agent, the solvent is composed of water and ethanol with a volume ratio of 1:1. The scanning electron microscopy and transmission electron microscopy images confirmed that the prepared MoS2 has a three-dimensional, hollow tubular structure. X-ray photoelectron spectroscopy combining with Raman spectroscopy proved that the prepared product contained pure phase MoS2.
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