Journal
SOLAR ENERGY MATERIALS AND SOLAR CELLS
Volume 159, Issue -, Pages 510-517Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.solmat.2016.10.008
Keywords
Nickel alloy; Molten salt; Transmission electron microscopy; EBSD; Oxidation; Stress corrosion cracking
Funding
- Australian Solar Thermal Research Initiative (ASTRI)
- Australian Government via Australian Renewable Energy Agency (ARENA)
- Science and Engineering Faculty, QUT
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Degradation of an Inconel 601 superalloy subjected to a eutectic mixture of carbonate salt at 450 degrees C was studied using advanced microscopy and microanalysis techniques. On the outside of the vessel, long term exposure to elevated temperature led to intergranular stress corrosion cracking via a stress assisted oxidation process. Elemental analysis verified diffusion controlled de-alloying of Ni and Cr from grain boundaries. Transmission electron microscopy showed that a (CrFeNiAl)(3)O-4 oxide phase was formed at grain boundaries as a result of oxygen penetration. Intergranular cracking appeared due to the presence of residual stresses and micro structural heterogeneities facilitated the crack branching.
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