Journal
RUSSIAN JOURNAL OF GENERAL CHEMISTRY
Volume 87, Issue 1, Pages 37-43Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S107036321701008X
Keywords
closo-decaborate anion; nitrilium derivatives; nucleophilic addition; amide oximes; oximes
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Funding
- Russian Foundation for Basic Research [16-03-00 573]
- Ministry of Education and Science of the Russian Federation [14.595.21.0001, RFMEFI59514X0001]
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A series of closo-decaborate anions containing an O-iminoacylamide oxime fragment were synthesized by nucleophilic addition of aromatic amide oximes to 2-propionitrilium closo-decaborate anion. The isolated compounds were characterized by IR, H-1, C-13-{H-1}, and B-11-{H-1} NMR, and mass spectra. The structure of ((PhP)-P-4)[2-B10H9NH= C(Et) ON= C(NH2)C6H4Me-2] was determined by single-crystal X-ray analysis.
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