Journal
POLYMER
Volume 109, Issue -, Pages 315-320Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.polymer.2016.12.052
Keywords
Porous organic polymers; Covalent organic frameworks; Cyclic voltammetry
Categories
Funding
- DST-SERB [SB/FT/CS-084/2014]
- DST-INSPIRE [DST/INSPIRE/04/2013/000449]
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Herein, we report the synthesis of 1,4-phenylenediamine based covalent triazine framework (CTF) by reacting cyanuric chloride with 1,4-phenylenediamine under basic conditions. The as synthesized polymeric framework was characterized by solid state C-13-CPMAS and N-15 NMR, FT-IR, Raman, SEM, TEM, UV-Vis and N-2 sorption isotherm. Commercially available glassy carbon electrode is modified with the as synthesized polymer and its electro catalytic activity towards the reduction of nitrobenzene and oxygen evolution reaction (OER) is studied. Performance of the bare CTF material resembles the performance of commercial GC (glassy carbon) electrode. (C) 2016 Elsevier Ltd. All rights reserved.
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