Journal
POLYMER
Volume 116, Issue -, Pages 412-422Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.polymer.2016.12.072
Keywords
Superhydrophobic; Polymethylhydroxysiloxane; Cetyl trimethylammonium bromide; Graphene oxide; Chloroform detection and separation
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Funding
- Post-Doc Development Program of Pusan National University, Korea
- National Research Foundation of Korea Grant - Ministry of Science, ICT & Future Planning, Korea, Acceleration Research Program [NRF-2014R1A2A1A11054584]
- Brain Korea 21 Plus Program [21A2013800002]
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Superhydrophobic mesoporous hybrid materials were synthesised by the in-situ self-hydroxylation and condensation of polymethylhydrosiloxane in ethanol and sodium hydroxide solutions in the presence of a cetyl trimethylammonium bromide (CTAB) as a surfactant and graphene oxide (GO). The samples were analysed by a range of characterisation techniques, such as Fourier-transform infrared and Raman spectroscopy, Si-29 cross polarisation magic angle spinning nuclear magnetic resonance spectroscopy, Xray diffraction, X-ray photoelectron spectroscopy, surface area analysis, high resolution scanning electron microscopy, and high resolution transmission electron microscopy. The superhydrophobic hybrid powder was used for the detection and separation of chloroform in water from water/chloroform mixtures. (C) 2016 Elsevier Ltd. All rights reserved.
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