Journal
ORGANIC LETTERS
Volume 19, Issue 4, Pages 862-865Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b00013
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Funding
- National Natural Science Foundation of China [21472086, 21531004]
- National Basic Research Program of China [2013CB922101]
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Base-promoted decarboxylative azo couplings of carboranyl carboxylic acids with diazo salts have been developed to provide trans-azocarboranes in high yields (up to 94%). This approach is simple, efficient, and compatible with various functional groups. Mechanistically, the coupling has been proven to proceed in a nonradical pathway, which is distinct from those classical decarboxylative couplings.
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