Journal
ORGANIC LETTERS
Volume 19, Issue 17, Pages 4440-4443Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b01919
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Funding
- National Key Research and Development Program of China [2016YFA0602900]
- National Natural Science Foundation of China [21490572, 21420102003]
- Pearl River S&T Nova Program of Guangzhou [201610010160]
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An efficient and robust protocol for the preparation of 3-substituted isocoumarins via palladium-catalyzed nucleophilic addition/oxidative annulation of bromoalkynes with benzoic acids has been developed. Remarkably, preliminary mechanistic studies indicated that the transformation might proceed via a stereo- and regioselective nucleophilic addition and C-H functionalization procedure.
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