Journal
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
Volume 684, Issue -, Pages 1-13Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2016.12.033
Keywords
High-pressure torsion; Mechanical behaviors; Defect-structures; Grain refinement
Categories
Funding
- National Natural Science Foundation of China (NSFC, China) [51374039]
- National Defense Key Basic Research and Development Program of China (Defense 973 Program, China) [613135]
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The high-pressure torsion method was employed to deform Ti-6Al-4V (TC4) alloy. The ambient temperature and high pressure were used to restrain the grain growth. Clear images showing the microstructure evolution of the deformed TC4 alloys were obtained using SEM, TEM and HRTEM. It was found that the HPT-deformed TC4 alloys contain a high density of dislocations and many defect structures. These dislocations were found to be generated on one or both sides of the elongated grains, and the dislocation lines were able to move across the elongated grains (mostly at similar to 60) to form an uncondensed dislocation wall. Although deformation twins did not appear in the alloys deformed at intermediate strains (gamma <= 23.1), quantities of (10-12) < 10-1-1 > tensile twins containing prismatic stacking faults were observed in the specimens deformed at a much larger plastic strain (gamma >= 157). The hardness-strain behaviors of the TC4 alloys were similar to those of pure Ti, which have a maximum hardness followed by a strain softening at large strains. In addition, the formation of the omega phase was suppressed due to the dissolution of substitutional Al and V. The alloy that received the highest levels of strain (gamma similar to 357) was found to have a nanoscale structure (similar to 49.41 nm) with non-equilibrium GBs, as well as an increased microhardness (similar to 424 HV) and yield strength (sigma(S)similar to 960 MPa). The effects of these defect-structures on the mechanical behaviors of a TC4 alloy are mainly determined by their structures sizes according to Hall-Petch relationship. However, the effect of this mechanism reduces at large strains due to the existing high-dense dislocations and non-equilibrium grain boundaries.
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