Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 82, Issue 17, Pages 9171-9174Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b01187
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- NNSFC [21472107, 21372142]
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A highly efficient synthesis of a-diazoketone was achieved by simply stirring the mixture of 1,3-diketone, TsN3, and MeNH2 in EtOH. It was a tandem reaction including a novel primary amine-catalyzed Regitz diazo transfer of 1,3-diketone and a novel primary amine-mediated C-C bond cleavage of 2-diazo-1,3-diketone.
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