☆ 4.7 Article

Electrocatalytic hydrogen gas generation by cobalt molybdenum disulfide (CoMoS2) synthesized using alkyl-containing thiomolybdate precursors

INTERNATIONAL JOURNAL OF HYDROGEN ENERGY (2017)

Journal

INTERNATIONAL JOURNAL OF HYDROGEN ENERGY

Volume 42, Issue 32, Pages 20669-20676

Publisher

PERGAMON-ELSEVIER SCIENCE LTD

DOI: 10.1016/j.ijhydene.2017.07.028

Keywords

Electrolysis; CoMoS2; Amine pretreated; Hydrogen

Categories

Chemistry, Physical Electrochemistry Energy & Fuels

Funding

NSF [CHE-1305124]

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Abstract

Cobalt molybdenum disulfide, (CoMoS2) catalysts are evaluated as active electrocatalysts for the production of hydrogen gas in acidic aqueous media. These highly-active hydrogen evolution reaction (HER) catalysts are obtained from pretreatment of ammonium tetrathiomolybdate (ATM) with different amines precursors, and characterized by x-ray diffraction (XRD), scanning electron microscopy (SEM) and their surface areas are determined by Brunauer-Emmett-Teller (BET) surface area analyses. Electrochemical studies indicate that these CoMoS2 materials exhibit enhanced catalytic performance for hydrogen gas production with overpotentials ranging from 0.127 to 0.144 V, which are significant less than CoMoS2 synthesized directly from ATM under the same synthetic techniques (0.173 V). These CoMoS2 catalysts are also stable in the presence of strong acidic media after a considerably long period of time (10 h) for maintaining their efficiencies for hydrogen gas evolution. (C) 2017 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved.

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R. van Doremalen, M. van Leeuwen, P. Vande Vyvre, D. Varga, Z. Varga, M. Varga-Kofarago, M. Vasileiou, A. Vasiliev, O. Vazquez Doce, V. Vechernin, A. Velure, E. Vercellin, S. Vergara Limon, L. Vermunt, R. Vertesi, M. Verweij, L. Vickovic, Z. Vilakazi, O. Villalobos Baillie, G. Vino, A. Vinogradov, T. Virgili, V. Vislavicius, A. Vodopyanov, B. Volkel, M. A. Volkl, K. Voloshin, S. A. Voloshin, G. Volpe, B. von Haller, I Vorobyev, N. Vozniuk, J. Vrlakova, B. Wagner, C. Wang, D. Wang, M. Weber, R. J. G. Weelden, A. Wegrzynek, S. C. Wenzel, J. P. Wessels, S. L. Weyhmiller, J. Wiechula, J. Wikne, G. Wilk, J. Wilkinson, G. A. Willems, B. Windelband, M. Winn, W. E. Witt, J. R. Wright, W. Wu, Y. Wu, R. Xu, A. K. Yadav, S. Yalcin, Y. Yamaguchi, K. Yamakawa, S. Yang, S. Yano, Z. Yin, I-K Yoo, J. H. Yoon, S. Yuan, A. Yuncu, V Zaccolo, C. Zampolli, H. J. C. Zanoli, F. Zanone, N. Zardoshti, A. Zarochentsev, P. Zavada, N. Zaviyalov, M. Zhalov, B. Zhang, S. Zhang, X. Zhang, Y. Zhang, V Zherebchevskii, Y. Zhi, N. Zhigareva, D. Zhou, Y. Zhou, J. Zhu, Y. Zhu, G. Zinovjev, N. Zurlo

Summary: We present the first measurement of event-by-event fluctuations in the kaon sector in Pb-Pb collisions at root S-NN = 2.76 TeV with the ALICE detector at the LHC. Our results show the magnitude of fluctuations of the relative yields of neutral and charged kaons, as well as the relative yields of charged kaons, as a function of collision centrality and selected kinematic ranges. Comparison with predictions and further discussion suggest a possible production of disoriented chiral condensates in central Pb-Pb collisions.

PHYSICS LETTERS B (2022)

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Article Astronomy & Astrophysics

KS0KS0 and KS0K± femtoscopy in pp collisions at √s=5.02and 13 TeV

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Mager, T. Mahmoud, A. Maire, M. Malaev, N. M. Malik, Q. W. Malik, S. K. Malik, L. Malinina, D. Mal'Kevich, D. Mallick, N. Mallick, G. Mandaglio, V Manko, F. Manso, V Manzari, Y. Mao, G. Margagliotti, A. Margotti, A. Marin, C. Markert, M. Marquard, N. A. Martin, P. Martinengo, J. L. Martinez, M. Martinez, G. Martinez Garcia, S. Masciocchi, M. Masera, A. Masoni, L. Massacrier, A. Mastroserio, A. M. Mathis, O. Matonoha, P. F. T. Matuoka, A. Matyja, C. Mayer, A. L. Mazuecos, F. Mazzaschi, M. Mazzilli, M. A. Mazzoni, J. E. Mdhluli, A. F. Mechler, Y. Melikyan, A. Menchaca-Rocha, E. Meninno, A. S. Menon, M. Meres, S. Mhlanga, Y. Miake, L. Micheletti, L. C. Migliorin, D. L. Mihaylov, K. Mikhaylov, A. N. Mishra, A. Modak, A. P. Mohanty, B. Mohanty, M. Mohisin Khan, M. A. Molander, Z. Moravcova, C. Mordasini, D. A. Moreira De Godoy, I Morozov, A. Morsch, T. Mrnjavac, V Muccifora, E. Mudnic, D. Muehlheim, S. Muhuri, J. D. Mulligan, A. Mulliri, M. G. Munhoz, R. H. Munzer, H. Murakami, S. Murray, L. Musa, J. Musinsky, J. W. Myrcha, B. Naik, R. Nair, B. K. Nandi, R. Nania, E. Nappi, A. F. Nassirpour, A. Nath, C. Nattrass, A. Neagu, A. Negru, L. Nellen, S. Nesbo, G. Neskovic, D. Nesterov, B. S. Nielsen, S. Nikolaev, S. Nikulin, V Nikulin, F. Noferini, S. Noh, P. Nomokonov, J. Norman, N. Novitzky, P. Nowakowski, A. Nyanin, J. Nystrand, M. Ogino, A. Ohlson, V. A. Okorokov, J. Oleniacz, A. C. Oliveira Da Silva, M. H. Oliver, A. Onnerstad, C. Oppedisano, A. Ortiz Velasquez, T. Osako, A. Oskarsson, J. Otwinowski, M. Oya, K. Oyama, Y. Pachmayer, S. Padhan, D. Pagano, A. Palasciano, J. Pan, S. Panebianco, J. Park, J. E. Parkkila, S. P. Pathak, R. N. Patra, B. Paul, H. Pei, T. Peitzmann, X. Peng, L. G. Pereira, H. Pereira DaCosta, D. Peresunko, G. M. Perez, S. Perrin, Y. Pestov, V. Petracek, M. Petrovici, R. P. Pezzi, S. Piano, M. Pikna, P. Pillot, O. Pinazza, L. Pinsky, C. Pinto, S. Pisano, M. Planinic, F. Pliquett, M. G. Poghosyan, B. Polichtchouk, S. Politano, N. Poljak, A. Pop, S. Porteboeuf-Houssais, J. Porter, V Pozdniakov, S. K. Prasad, R. Preghenella, F. Prino, C. A. Pruneau, I Pshenichnov, M. Puccio, S. Qiu, L. Quaglia, R. E. Quishpe, S. Ragoni, A. Rakotozafindrabe, L. Ramello, F. Rami, S. A. R. Ramirez, A. G. T. Ramos, T. A. Rancien, R. Raniwala, S. Raniwala, S. S. Rasanen, R. Rath, I Ravasenga, K. F. Read, A. R. Redelbach, K. Redlich, A. Rehman, P. Reichelt, F. Reidt, H. A. Reme-ness, Z. Rescakova, K. Reygers, A. Riabov, V Riabov, T. Richert, M. Richter, W. Riegler, F. Riggi, C. Ristea, M. Rodriguez Cahuantzi, K. Roed, R. Rogalev, E. Rogochaya, T. S. Rogoschinski, D. Rohr, D. Rohrich, P. F. Rojas, S. Rojas Torres, P. S. Rokita, F. Ronchetti, A. Rosano, E. D. Rosas, A. Rossi, A. Roy, P. Roy, S. Roy, N. Rubini, O. Rueda, D. Ruggiano, R. Rui, B. Rumyantsev, P. G. Russek, R. Russo, A. Rustamov, E. Ryabinkin, Y. Ryabov, A. Rybicki, H. Rytkonen, W. Rzesa, O. A. M. Saarimaki, R. Sadek, S. Sadovsky, J. Saetre, K. Safarik, S. K. Saha, S. Saha, B. Sahoo, P. Sahoo, R. Sahoo, S. Sahoo, D. Sahu, P. K. Sahu, J. Saini, S. Sakai, M. P. Salvan, S. Sambyal, V Samsonov, T. B. Saramela, D. Sarkar, N. Sarkar, P. Sarma, V. M. Sarti, M. H. P. Sas, J. Schambach, H. S. Scheid, C. Schiaua, R. Schicker, A. Schmah, C. Schmidt, H. R. Schmidt, M. O. Schmidt, M. Schmidt, N. Schmidt, A. R. Schmier, R. Schotter, J. Schukraft, K. Schwarz, K. Schweda, G. Scioli, E. Scomparin, J. E. Seger, Y. Sekiguchi, D. Sekihata, I Selyuzhenkov, S. Senyukov, J. J. Seo, D. Serebryakov, A. Sevcenco, T. J. Shaba, A. Shabanov, A. Shabetai, R. Shahoyan, W. Shaikh, A. Shangaraev, A. Sharma, H. Sharma, M. Sharma, N. Sharma, S. Sharma, U. Sharma, A. Shatat, O. Sheibani, K. Shigaki, M. Shimomura, S. Shirinkin, Q. Shou, Y. Sibiriak, S. Siddhanta, T. Siemiarczuk, T. F. Silva, D. Silvermyr, T. Simantathammakul, G. Simonetti, B. Singh, R. Singh, R. Singh, R. Singh, V. K. Singh, V Singhal, T. Sinha, B. Sitar, M. Sitta, T. B. Skaali, G. Skorodumovs, M. Slupecki, N. Smirnov, R. J. M. Snellings, C. Soncco, J. Song, A. Songmoolnak, F. Soramel, S. Sorensen, I Sputowska, J. Stachel, I Stan, P. J. Steffanic, S. F. Stiefelmaier, D. Stocco, I Storehaug, M. M. Storetvedt, P. Stratmann, C. P. Stylianidis, A. A. P. Suaide, C. Suire, M. Sukhanov, M. Suljic, R. Sultanov, V Sumberia, S. Sumowidagdo, S. Swain, A. Szabo, I Szarka, U. Tabassam, S. F. Taghavi, G. Taillepied, J. Takahashi, G. J. Tambave, S. Tang, Z. Tang, J. D. Tapia Takaki, M. Tarhini, M. G. Tarzila, A. Tauro, G. Tejeda Munoz, A. Telesca, L. Terlizzi, C. Terrevoli, G. Tersimonov, S. Thakur, D. Thomas, R. Tieulent, A. Tikhonov, A. R. Timmins, M. Tkacik, A. Toia, N. Topilskaya, M. Toppi, F. Torales-Acosta, T. Tork, A. Trifiro, S. Tripathy, T. Tripathy, S. Trogolo, V Trubnikov, W. H. Trzaska, T. P. Trzcinski, A. Tumkin, R. Turrisi, T. S. Tveter, K. Ullaland, A. Uras, M. Urioni, G. L. Usai, M. Vala, N. Valle, S. Vallero, L. V. R. van Doremalen, M. van Leeuwen, P. Vande Vyvre, D. Varga, Z. Varga, M. Varga-Kofarago, M. Vasileiou, A. Vasiliev, O. Vazquez Doce, V. Vechernin, A. Velure, E. Vercellin, S. Vergara Limon, L. Vermunt, R. Vertesi, M. Verweij, L. Vickovic, Z. Vilakazi, O. Villalobos Baillie, G. Vino, A. Vinogradov, T. Virgili, V. Vislavicius, A. Vodopyanov, B. Volkel, M. A. Volkl, K. Voloshin, S. A. Voloshin, G. Volpe, B. von Haller, I Vorobyev, N. Vozniuk, J. Vrlakova, B. Wagner, C. Wang, D. Wang, M. Weber, R. J. G. Weelden, A. Wegrzynek, S. C. Wenzel, J. P. Wessels, J. Wiechula, J. Wikne, G. Wilk, J. Wilkinson, G. A. Willems, B. Windelband, M. Winn, W. E. Witt, J. R. Wright, W. Wu, Y. Wu, R. Xu, A. K. Yadav, S. Yalcin, Y. Yamaguchi, K. Yamakawa, S. Yang, S. Yano, Z. Yin, I-K Yoo, J. H. Yoon, S. Yuan, A. Yuncu, V Zaccolo, C. Zampolli, H. J. C. Zanoli, N. Zardoshti, A. Zarochentsev, P. Zavada, N. Zaviyalov, M. Zhalov, B. Zhang, S. Zhang, X. Zhang, Y. Zhang, V Zherebchevskii, Y. Zhi, N. Zhigareva, D. Zhou, Y. Zhou, J. Zhu, Y. Zhu, G. Zinovjev, N. Zurlo

Summary: Femtoscopic correlations between the particle pair combinations (KSKS0)-K-0 and (KSK +/-)-K-0 are investigated in pp collisions at root s= 5.02 and 13 TeV using the ALICE experiment. The boson source parameters for both pair combinations are obtained by fitting models based on Gaussian size distributions to the measured two-particle correlation functions. The (KSKS0)-K-0 analysis incorporates quantum statistics and strong final-state interactions involving the f(0)(980) and a(0)(980) resonances, while the (KSK +/-)-K-0 analysis considers only the final-state interaction through the a(0) resonance. The extracted source parameters from this study are compared with previously published values from pp collisions at root s = 7 TeV, and the different pair combinations show consistency. The observed stronger correlation strength in (KSKS0)-K-0 suggests that the a(0) resonance could be a tetraquark state of the form (q(1), (q(2)) over bar, s, (s) over bar), where q(1) and q(2) are u or d quarks.

PHYSICS LETTERS B (2022)

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Article Engineering, Environmental

Biofilm Control in Flow-Through Systems Using Polyvalent Phages Delivered by Peptide-Modified M13 Coliphages with Enhanced Polysaccharide Affinity

Ruonan Sun, Pingfeng Yu, Pengxiao Zuo, Dino Villagran, Jacques Mathieu, Pedro J. J. Alvarez

Summary: This study explores the use of engineered bacteriophage M13 to enhance biofilm affinity and precise delivery of polyvalent phages in water distribution systems. The modified M13 shows higher affinity and effectiveness in delivering polyvalent phages to biofilms, resulting in reduced bacterial biomass, biofilm surface coverage, and biofilm regrowth.

ENVIRONMENTAL SCIENCE & TECHNOLOGY (2022)

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Article Chemistry, Multidisciplinary

Enhanced Gas Adsorption on Cu3(BTC)2 Metal-Organic Framework by Post-Synthetic Cation Exchange and Computational Analysis

Jose M. Veleta, Roy A. Arrieta, Yanyu Wu, Miguel A. Baeza, Karen Castaneda, Dino Villagran

Summary: Increased gas adsorption was achieved in post-synthetically modified metal-organic frameworks (MOFs) of HKUST-1 type through a partial cation exchange process. The manipulation of post-synthetic conditions exhibited high tunability in site substitution and gas adsorption properties. The study conducted post-synthetic modification of Cu-3(BTC)(2) by exposure to TM2+ solutions (TM= Mn, Fe, Co, Ni) at different time intervals, and the crystal structure, composition, and morphology were analyzed. The results showed that the gas adsorption capacity could be enhanced by forming defects in the crystal structure during the cation exchange process.

LANGMUIR (2023)

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Article Astronomy & Astrophysics

Pauli Exclusion Classical Potential for Intermediate-Energy Heavy-Ion Collisions

Claudio O. Dorso, Guillermo Frank, Jorge A. Lopez

Summary: This article presents a classical potential used to describe nucleon-nucleon interactions at intermediate energies. The potential, depending on the relative momentum of the colliding nucleons, can simulate interactions at low momentum transfer mimicking the Pauli exclusion principle. By combining the potential with molecular dynamics, the study explores finite nuclei, including their binding energy, radii, symmetry energy, and a case analysis of collisions.

UNIVERSE (2023)

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Review Engineering, Environmental

Computational Chemistry as Applied in Environmental Research: Opportunities and Challenges

Christian Sandoval-Pauker, Sheng Yin, Alexandria Castillo, Neidy Ocuane, Diego Puerto-Diaz, Dino Villagran

Summary: The constant development of computer systems and infrastructure has enabled computational chemistry to play a crucial role in environmental chemistry research. This review article highlights the various applications of computational chemistry techniques, such as quantum and classical mechanical calculations, in modeling and understanding environmental systems. It also discusses the recent introduction of artificial intelligence and machine learning techniques and their potential impact on the field.

ACS ES&T ENGINEERING (2023)

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Review Chemistry, Inorganic & Nuclear

Molecular inspired electrocatalyst materials for environmental remediation

Jonathan J. Calvillo Solis, Alexandria Castillo, Sheng Yin, Christian Sandoval-Pauker, Neidy Ocuane, Diego Puerto-Diaz, Nasim Jafari, Dino Villagran

Summary: This review evaluates the advances in the application of molecularly-inspired catalysts for the electrochemical degradation of various pollutants, and discusses the impact of molecular structure on electrochemical parameters. The potential applications of electrochemical degradation for poly- and per-fluoroalkyl substances are briefly mentioned, and the utilization of computational chemistry in investigating catalytic sites and reaction mechanisms is also discussed.

INORGANIC CHEMISTRY FRONTIERS (2023)

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Article Chemistry, Multidisciplinary

Free-base porphyrin polymer for bifunctional electrochemical water splitting

Yulu Ge, Zhenhua Lyu, Mariana Marcos-Hernandez, Dino Villagran

Summary: This article reports a metal-free porphyrin-based two-dimensional crystalline covalent organic polymer with outstanding bifunctional electrocatalytic performance for water splitting, providing a sustainable alternative to high-quality metal electrocatalysts.

CHEMICAL SCIENCE (2022)

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Article Chemistry, Physical

Cobalt porphyrin intercalation into zirconium phosphate layers for electrochemical water oxidation

Isabel Barraza Alvarez, Yanyu Wu, Joel Sanchez, Yulu Ge, Mario V. Ramos-Garces, Tong Chu, Thomas F. Jaramillo, Jorge L. Colon, Dino Villagran

Summary: Intercalating CoTcPP into ZrP layers enhances the efficiency and catalytic stability of water oxidation reactions, with the electrochemical behavior being superior to pristine α-ZrP material.

SUSTAINABLE ENERGY & FUELS (2021)

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