4.2 Article

A Johann-type X-ray emission spectrometer at the Rossendorf beamline

Journal

JOURNAL OF SYNCHROTRON RADIATION
Volume 23, Issue -, Pages 836-841

Publisher

INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600577516004483

Keywords

X-ray emission spectrometer; Johann geometry; XANES; HERFD; XES; RIXS; actinides

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This paper gives a detailed description, including equations, of the Johann-type X-ray emission spectrometer which has been recently installed and tested at the Rossendorf beamline (ROBL) of the European Synchrotron Radiation Facility. The spectrometer consists of a single spherically bent crystal analyzer and an avalanche photodiode detector positioned on the vertical Rowland cycle of 1 m diameter. The hard X-ray emission spectrometer (similar to 3.5-25 keV) operates at atmospheric pressure and covers the Bragg angles of 65 degrees-89 degrees. The instrument has been tested at high and intermediate incident energies, i.e. at the Zr K-edge and at the Au L-3-edge, in the second experimental hutch of ROBL. The spectrometer is dedicated for studying actinides in materials and environmental samples by high-energy-resolution X-ray absorption and X-ray emission spectroscopies.

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