4.5 Article

Ultrasound-assisted one-pot multi-component synthesis of 2-pyrrolidinon-3-olates catalyzed by Co3O4@SiO2 core-shell nanocomposite

Journal

GREEN CHEMISTRY LETTERS AND REVIEWS
Volume 9, Issue 3, Pages 156-165

Publisher

TAYLOR & FRANCIS LTD
DOI: 10.1080/17518253.2016.1204013

Keywords

Multi-component reaction; ultrasound irradiation; 2-pyrrolidinon-3-olates; Co3O4@SiO2; Nanocomposite

Funding

  1. Islamic Azad University, Qom Branch, Qom, I. R. Iran [2014-13929]

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2-pyrrolidinon-3-olates were synthesized via one-pot four-component reaction of 2-aminobenzothiazole, aromatic aldehydes, dimethyl acetylenedicarboxylate and morpholine/piperidine in the presence of Co3O4@SiO2 core-shell nanocomposite as catalyst under ultrasound irradiation. The protocol offers several such advantages as high yields, short reaction time and mild reaction conditions with reusability of the catalyst. The core-shell nanocomposite was also prepared using ultrasound irradiation and the structure and magnetic properties were fully characterized by TEM, FE-SEM, XRD, EDX, FT-IR and VSM analysis. [GRAPHICS] .

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