Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 20, Issue 4, Pages 831-835Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.oprd.6b00044
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Funding
- CatchBio Project [053.70.376]
- Marie S. Curie-foundation for a Marie Curie-Intra-European Fellowship [622415]
- Dutch Science Foundation (NWO) via an ECHO grant [713.013.001]
- VIDI grant [14150]
- European Union for a Marie Curie CIG grant [333659]
- ERC Advanced Grant [267443]
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Herein, the first continuous cross-dehydrogenative homocoupling of an unactivated arene using oxygen as sole oxidant is reported. Employing micro reactor technology which enables the use of elevated temperatures and pressures leads to a boost of the catalytic reaction. Hence, a major reduction in reaction time is achieved. Due to the significance as precursor for MOFs as well as high-tech and high-value polymers, the study focused on the production of 3,4,3',4'-tramethyl-biphenyl.
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