Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 20, Issue 2, Pages 517-524Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.oprd.5b00363
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Funding
- NSERC (Canada)
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An automated collection/diversion device for high-pressure continuous flow synthesis is introduced. Integration of sampling and collection functions with decision-making capabilities to handle process disruptions is detailed. A device to mitigate pressure swing effects of reciprocal pump systems is also described. System performance is evaluated by simulating fast and slow chemical processes and Change of critical reaction parameters, including the ones that involve flow catalysis.
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