Journal
ORGANIC LETTERS
Volume 18, Issue 10, Pages 2379-2382Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b00843
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Funding
- Natural Science Foundation of China [21372174, 21542015]
- PAPD
- Soochow University
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Palladium-catalyzed intramolecular Heck reaction and aminopalladation of N-(2-(1-phenylvinyl)phenyl)-aniline for the efficient synthesis of dihydroindeno [1,2,3-kl]acridines and 3-arylindoles via tuning of the phosphine ligands and solvents under two optimized conditions are reported. The reaction follows a 1,4-Pd migration, aminopalladation, C(sp(2))-H activation, as well as five- and six-membered-ring fusion to form different products. The dihydroindeno[1,2,3-kl]acridine derivatives showed higher triplet energy (E-T) levels than common blue phosphorescent dopant and may serve as good host candidates for blue triplet emitters.
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