Journal
ORGANIC LETTERS
Volume 18, Issue 9, Pages 2012-2015Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b00618
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Funding
- NSFC [21402046, 21172060, 21472039]
- Hunan Provincial Natural Science Foundation of China [13JJ2018]
- Hunan Province Science and Technology Project [2015JC3052]
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A practical and straightforward access to pyrazolo [3,4-c]quinolines by molecular sieve mediated dehydrogenative [2 + 2 + 1] heteroannulation of N-(o-alkenylaryl)imines with aryldiazonium salts is described using a spa-hybrid carbon atom as a one-carbon unit. The reaction enables the formation of three new chemical bonds, a C-C bond and two C-N bonds, in a single reaction and features simple operation and excellent functional group tolerance.
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