Journal
ORGANIC LETTERS
Volume 18, Issue 16, Pages 4048-4051Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b01903
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Funding
- National Science Foundation [CHE-1507344]
- National Institutes of Health [GM098141]
- Louisiana Board of Regents [LEQSF(2012-17)-GF-SREB-03]
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1507344] Funding Source: National Science Foundation
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An efficient, four-step synthesis of a range of water-soluble deep-cavity cavitands is presented. Key to this approach are octahalide derivatives (4, X = Cl or Br) that allow a range of water-solubilizing groups' to be added to the outer surface of the core host structure. In many cases, the conversion of the starting dodecol (1) resorcinarene to the different cavitands avoids any chromatographic procedures.
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