Journal
ORGANIC LETTERS
Volume 18, Issue 4, Pages 856-859Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.6b00142
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Funding
- National Basic Research Program of China [2015CB931900, 2012CB215500]
- National Natural Science Foundation of China [21372246, 21421002]
- Shanghai City [15XD1504400]
- Chinese Academy of Sciences
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A one-pot trifluoromethylthiolation-iodination of arynes with trifluoromethylthiosilver (AgSCF3) and 1-iodophenylacetylene is described. This protocol allows rapid construction of o-trifluoromethylthiolated arene building blocks in moderate yields. These products were found to be excellent precursors for Yagupolskii-Umemoto-type electrophilic trifluoromethylation reagents.
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