Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 14, Issue 23, Pages 5317-5321Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ob00925e
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Funding
- National Natural Science Foundation of China [21502049, 51573040]
- Planned Science and Technology Project of Hunan Province, China [2015WK3003]
- Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation [2015CL03]
- Changsha University of Science & Technology, P.R. China
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Fast sulfonylation of pyridine/quinoline N-oxides induced by iodine is demonstrated herein. The regioselective protocol occurs under metal-free conditions in a short reaction time (10 min), exhibiting high efficiency (up to 92% yield) and good compatibility (up to 33 examples). A gram-scale reaction was conducted with only a slight loss of production.
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