Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 14, Issue 30, Pages 7275-7281Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ob01374k
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Funding
- National Natural Science Foundation of China [NSFC 21404096, U1463202]
- Fundamental Research Funds for the Central Universities of China [WK2060190026, WK3430000001]
- Anhui Provincial Natural Science Foundation [1608085MB24]
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Oxychlorination of alkenyl oximes is harder compared to the analogous oxybromination or oxyiodination because of the difficulty associated with the formation of chlorine cations or radicals. A transition-metal-free oxychlorination of alkenyl oximes has been developed, using t-BuONO as a dual oxidant and AlCl3 as a chlorine source. This convenient and practical method has been used to construct chloroisoxazolines in moderate to good yields, whereas N-chlorosuccinimide (NCS) failed to promote this reaction.
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