Journal
CHEMISTRY LETTERS
Volume 44, Issue 11, Pages 1598-1600Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.150739
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Funding
- MEXT
- JSPS
- JST, Japan
- Grants-in-Aid for Scientific Research [25288048, 14J00760] Funding Source: KAKEN
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The rhodium-catalyzed intramolecular Ar-H/Ar-H coupling of 3-phenoxybenzoic acids proceeds smoothly, accompanied by double C-H bond cleavage at the 2- and 2'-positions, to produce dibenzofuran-l-carboxylic acid derivatives. Related tetra- and pentacyclic molecules can also be readily constructed by the present procedure. A reaction mechanism involving 1,4-rhodium(III) migration is proposed.
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