Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 16, Pages 3438-3441Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc09775k
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Funding
- Defence Threat Reduction Agency [HDTRA1-11-1-0034]
- ONR [NOOO14-12-1-0536]
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An efficient route to polyiodopyrazoles, 3,4,5-triiodopyrazole (1), 1-methyl-3,4,5-triiodopyrazole (2) and 1-diiodomethyl-3,4,5-triiodo-pyrazole (3), opens the door to prospective biocides. Nitration of 1 and 2 gives the previously inaccessible compounds, 3,4-dinitro-5-iodopyrazole (4), and 3,4-dinitro-5-iodo-1-methylpyrazole (5), respectively. These synthetic pathways will open many fronts for pyrazole chemistry.
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