Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 51, Pages 10276-10279Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc02374b
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Funding
- CSIR, New Delhi
- DST New Delhi [SB/S1/OC-42/2014]
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A novel, I-2 catalyzed regio-and stereodivergent vicinal azidohydroxylation of alkenes leading to 1,2-azidoalcohols in high yields (up to 92%) and excellent dr (up to 98%) has been developed. This unprecedented transformation employs NaN3 and DMF as N-and O-nucleophiles respectively. The role of DMF as the O-source in the reaction has been unequivocally proven by O-18 labelling studies.
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