Article
Materials Science, Multidisciplinary
Shuhui Lv, Qiang Yang, Xiaoling Lv, Fanzhi Meng, Xin Qiu
Summary: A ZK60 alloy was prepared by conventional direct extrusion at a reduced temperature, resulting in finer DRXed grains with stronger fiber texture and more abundant lath-like sub-grains. After aging, nanosized precipitates formed in both DRXed and non-recrystallized grains, while coarse MgZn2 particles precipitated on sub-grain boundaries. The aged ZK60 alloy exhibited significantly high ultimate compressive strength, excellent strength-ductility balance, and a weakened tension-compression yield strength asymmetry.
MATERIALS & DESIGN
(2023)
Article
Metallurgy & Metallurgical Engineering
Kai Guan, Daisuke Egusa, Eiji Abe, Jinghuai Zhang, Xin Qiu, Qiang Yang, Jian Meng
Summary: The effect of Gd content on the microstructure and tensile properties of as-cast Mg-Sm-Zn-Zr alloy was investigated. The addition of Gd inhibited the segregation behavior of Zn in the Mg3Sm phase and improved the tensile yield stress of the alloy. Gd-modified alloys exhibited significant age-hardening effect, attributed to the high-volume fraction and high density nano-scale precipitates.
JOURNAL OF MAGNESIUM AND ALLOYS
(2022)
Article
Nanoscience & Nanotechnology
Prithvi D. Awasthi, Priyanka Agrawal, Ravi Sankar Haridas, Rajiv S. Mishra, Michael T. Stawovy, Scott Ohm, Aidin Imandoust
Summary: This study evaluated the compatibility of C103 alloy for laser-based additive manufacturing, successfully fabricating crack-free AM specimens with relative densities exceeding 99%. Analysis using transmission electron microscopy showed that the high dislocation density and formation of dislocation cell structures in AM specimens led to higher strength levels.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2022)
Article
Materials Science, Multidisciplinary
Yan Liu, Jinshan Li, Bin Tang, Lin Song, William Yi Wang, Dong Liu, Rui Yang, Hongchao Kou
Summary: The decomposition mechanism of (alpha(2) /gamma) lamellae was investigated using transmission electron microscopy (TEM) and high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM) techniques. The results revealed the facilitated alpha(2)->ss phase transformation and the formation of ellipsoidal omega(o) particles. The mechanism of the lath-shaped omega(o) phase was attributed to both element segregation and strain accommodation caused by the ss o precipitate in alpha(2) lamellae. These findings provide insights into the decomposition mechanism of (alpha(2)/gamma) lamellae and have implications for controlling microstructures and improving the performance of ss-solidified gamma-TiAl alloys.
Article
Chemistry, Physical
Xu Liu, Lin Song, Andreas Stark, Daria Lazurenko, Florian Pyczak, Tiebang Zhang
Summary: The study investigates the precipitation behavior of the omega(o) phase and creep properties of a Ti-45Al-9Nb-0.5B alloy at intermediate temperatures. It shows that the imposed stress contributes to the nucleation and growth of the omega(o) phase, which can reduce the creep resistance of the material. Additionally, dynamic recrystallization is identified as a primary cause of microstructural degradation.
JOURNAL OF ALLOYS AND COMPOUNDS
(2021)
Article
Chemistry, Physical
Kai Chen, Qunbo Fan, Jiahao Yao, Lin Yang, Shun Xu, Yu Gao, Wei Lei
Summary: This study investigates the stress-induced alpha phase transformation in Ti-5Al-2.5Cr-5Mo-1Sn alloy by adjusting the heat treatment process. The results show that the stress-induced alpha phase exhibits a higher degree of plastic deformation compared to the beta matrix and demonstrates a strong strain partitioning effect during the stretching process, improving the material's ductility.
JOURNAL OF ALLOYS AND COMPOUNDS
(2022)
Article
Nanoscience & Nanotechnology
Jin-Sung Hong, Young-Kook Lee
Summary: The mechanism of dislocation multiplication during thermally-induced gamma austenite <-> e martensite transformation in the Fe-17Mn alloy was investigated using an in-situ transmission electron microscope. Dislocations were introduced in gamma at grain boundaries and inside the grains during thermally - induced gamma <-> e transformations. These dislocations played different roles, including constituting e martensite and returning to grain boundaries during e -> gamma reverse transformation, as well as being introduced by plastic deformation during gamma <-> e transformations.
SCRIPTA MATERIALIA
(2023)
Article
Chemistry, Physical
A. Semenyuk, M. Klimova, D. Shaysultanov, G. Salishchev, S. Zherebtsov, N. Stepanov
Summary: The addition of nitrogen to a CoCrFeMnNi high-entropy alloy improves its structure and mechanical properties, enhancing strength and ductility. Subsequent annealing can further optimize the material's performance.
JOURNAL OF ALLOYS AND COMPOUNDS
(2021)
Article
Nanoscience & Nanotechnology
Qiang Lu, Jingjing Hu, Tong Yang, Yucheng Wang, Yao Xiao, Xingwu Li, Namin Xiao, Jinsan Wang, Zhixiu Wang, Hai Li, Liya Li, Kai Li, Yong Du
Summary: In heat-resistant Al-Cu-Mg-Ag alloys, the presence of AgMg segregation layer on omega phase ensures its high thermal stability. It has been proved that an increase in Ag content can promote the precipitation of omega, even in an Al-Cu-Mg-Ag-Si alloy with a Mg/Si mass ratio around 1.7. The key point is to obtain an Ag/Mgexcess atomic ratio greater than 1 in the supersaturated solid solution. Although the fine precipitation of omega increases the total volume fraction of precipitates and yield strength, their quick coarsening at high temperature leads to a more pronounced strength loss.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2023)
Article
Materials Science, Multidisciplinary
Jacob Obitso Nielsen, Flemming Bjerg Grumsen, Karen Pantleon
Summary: This study investigates the evolution of crystallite size and microstrain in ferrite in real time using energy-dispersive synchrotron diffraction, providing insights into the thermal stability and phase transformations of iron-carbon coatings.
MATERIALS CHARACTERIZATION
(2021)
Article
Chemistry, Physical
M. Klimova, D. Shaysultanov, A. Semenyuk, S. Zherebtsov, N. Stepanov
Summary: The study investigated the effect of carbon content on the phase composition, microstructure, and mechanical properties of thermomechanically processed CoCrFeMnNi high-entropy alloys. Results showed that increasing carbon content led to an increase in strength and a slight decrease in ductility. At low temperatures, the alloy with 2.0 at.% carbon demonstrated an attractive combination of mechanical properties.
JOURNAL OF ALLOYS AND COMPOUNDS
(2021)
Article
Nanoscience & Nanotechnology
Hui-Dong Qian, Jung Tae Lim, Jong-Woo Kim, Yang Yang, Kyung Mox Cho, Jihoon Park, Chul-Jin Choi
Summary: This study successfully produced high density sintered Sm(Fe0.8Co0.2)(11)Ti bulk magnets using a newly developed high pressure pressing method. The purity of the hard magnetic ThMn12 phase in the bulk magnet was over 97 wt.%. The phase transformation behavior from amorphous to ThMn12 phase during heat treatment was systematically investigated, achieving high remanent magnetization and maximum energy product. The achieved maximum energy product in the bulk magnet is the highest reported among all SmFe12-based bulk magnets.
SCRIPTA MATERIALIA
(2021)
Article
Materials Science, Multidisciplinary
G. H. Cao, Z. Zhang, X. Li, W. Skrotzki, E. Mueller, R. Schneider, D. Gerthsen
Summary: The study found that nickel plays an important role in stabilizing the high-temperature Pt3Al(h) phase, while phases such as Ni2PtAl and NiPt2Al have been observed and confirmed experimentally. The phase transition and formation mechanisms involved during cooling have also been analyzed.
Article
Metallurgy & Metallurgical Engineering
Fanzhi Meng, Shuhui Lv, Qiang Yang, Xin Qiu, Zixiang Yan, Qian Duan, Jian Meng
Summary: This study investigated the components and crystal structures of intermetallic phases in a gravity die-cast Mg-6.0Zn-1.5Nd-0.5Zr alloy using transmission electron microscopy. The results revealed multiple intermetallic phases and various internal faults in the alloy. The study also revealed new orientation relationships between different intermetallic phases.
JOURNAL OF MAGNESIUM AND ALLOYS
(2022)
Article
Materials Science, Multidisciplinary
John Nutter, Jiahui Qi, Hussein Farahani, W. Mark Rainforth, Sybrand van der Zwaag
Summary: This study utilized in situ transmission electron microscopy to observe the growth of bainitic ferrite in Fe-0.3C-3Mn-1.5Si-0.15Mo steel at 300 degrees C. The study achieved a higher spatio-temporal resolution compared to previous studies. The growth rate of bainitic ferrite exhibited significant variations, with the highest rate exceeding 30,000 nm/s. The observations revealed both sheaves with visible sub units and individual laths during growth.
Article
Chemistry, Physical
Ghulam Abbas Ashraf, Raqiqa Tur Rasool, Jing Chen, Lianjie Li, Muhammad Hassan, Jazib Ali, Lanting Zhang, Hai Guo
Summary: Element engineering in the Mhexaferrite system has been shown to boost catalytic activation effectively. This study used a novel LaCr substituted Mhexaferrite photocatalyst for degrading organic pollutants in water under LED irradiation, achieving more efficient results compared to conventional Mhexaferrite NPs.
JOURNAL OF MOLECULAR LIQUIDS
(2022)
Article
Engineering, Multidisciplinary
Xiaoping Wang, Weiwei Dong, Peng Zhang, Haoqi Tang, Lanting Zhang, Tieying Yang, Peng Liu, Hong Wang, X. -d. Xiang
Summary: This work demonstrates high-throughput powder X-ray diffraction using a white X-ray beam and an energy-dispersive detector array. The results show consistent diffraction patterns with angle-resolved XRD, which is necessary for analyzing crystal structures of unknown samples.
Article
Chemistry, Physical
Tieqiao Zhang, Shengsheng Liu, Zhongwei Wu, Lanting Zhang, Rong Yu
Summary: In this study, a high-temperature short-term annealing process was used to simultaneously improve the coercivity, remanence, and squareness factor of hot-deformed Nd-Fe-B magnets. The increase in coercivity was attributed to the melting and infiltration of the Nd-6(Fe,Co)(13)Ga phase. The slightly anisotropic growth of Nd2Fe14B grains resulted in improved grain alignment and enhanced remanence. The addition of a small amount of Co element significantly reduced the melting point of the Nd6Fe13Ga phase. A balance between infiltration within the powder flakes and grain growth was achieved, leading to the simultaneous improvement of coercivity, remanence, and squareness factor in hot-deformed Nd-Fe-B samples.
JOURNAL OF ALLOYS AND COMPOUNDS
(2022)
Article
Materials Science, Multidisciplinary
Xiaozhen Wang, Yishi Su, Xiaoshu Wang, Kan Liu, Lanting Zhang, Qiubao Ouyang, Di Zhang
Summary: In this study, the W-Cu composite coating was deposited on graphite flakes, and the GFs(W-Cu)/Cu composites were prepared by vacuum hot-pressing sintering. The interfacial bonding changed from mechanical connection to mechanical-metallurgical synergy, resulting in improved mechanical properties, thermal conductivity, and coefficient of thermal expansion of the composites.
MATERIALS & DESIGN
(2022)
Article
Materials Science, Multidisciplinary
Yuanxun Zhou, Yongchao Rao, Lanting Zhang, Shenghong Ju, Hong Wang
Summary: In this work, a kernel ridge regression (KRR) model was developed to accurately predict the Vegard's law factor (VLF) and volume size factor (SF) of binary substitutional metallic solid solutions (BSMSS). The model achieved good performance using 409 published entries and elemental descriptors. Additionally, an explicit expression was learned to explain the electronic coupling effect.
Article
Nanoscience & Nanotechnology
Yao Lu, Kai Zhang, Bingbing Zhao, Xianping Dong, Lanting Zhang
Summary: In this study, two high-entropy alloys were designed to explore the possibility of replacing expensive Co with Ni. The aging treatment at different temperatures showed that both alloys exhibited a good balance of strength and ductility at room temperature. The Al0.3CrFeNi2 alloy showed higher yield strength and lower elongation compared to the Al0.3CoCrFeNi alloy after aging at 550 degrees C. The difference in mechanical properties can be attributed to the volume fraction difference of L12 and M23C6 phases in the two alloys.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2022)
Article
Metallurgy & Metallurgical Engineering
Xin Zou, Cunli Liu, Muyang Deng, Ji Chen, Lanting Zhang, Ke Chen
Summary: Abnormal grain growth (AGG) commonly occurs during the post-weld heat treatment (PWHT) of friction stir welded (FSWed) AA6061, reducing joint strength and limiting its usage in superplastic forming. In this research, a new welding method with the introduction of a ball-milled Al-Ti powder mixture into the stir zone effectively inhibited AGG during PWHT. Microscopic characterizations revealed the evolution of the powder mixture into different particle formations and Al3Ti new phase. Quantitative analysis confirmed the increases in particle number and average size, validating the grain growth model and the enhanced particle pinning effect for AGG inhibition.
ACTA METALLURGICA SINICA-ENGLISH LETTERS
(2023)
Article
Chemistry, Physical
Cai Chen, Xinyi Ji, Jianhao Wang, Mei Liu, Yao Lu, Xiaoping Wang, Aimin Zhang, Li Chen, Xianping Dong, Lanting Zhang, Hong Wang
Summary: Fe-X-Ni (X 1/4 Cr, W and V) combinatorial thin-film materials chips were fabricated and characterized to establish the composition-phase-magnetic properties relationships. The results showed that saturation magnetization decreases with increasing dopped elements content and is influenced by grain size and texture. Comparing the Fe-X-Ni systems, different alloying elements lead to diverse magnetic properties due to the orientation and crystallinity of the fcc phase. The effect of heat treatment on magnetic properties indicates a close relationship between saturation magnetization and duration of heat treatment.
JOURNAL OF MATERIOMICS
(2023)
Article
Materials Science, Multidisciplinary
Mei Liu, Lanting Zhang, Bingbing Zhao, Fugang Chen, Xianshuang Xia, Yongjiang Yu, Hajime Yamamoto, Kazuhiro Ito
Summary: In this study, the plastic deformation behavior of Nd2Fe14B matrix grains was investigated by uniaxial compression. The stress exponent n and apparent activation energy Q were found to increase as the c-axis rotation increased from 0 degrees to 90 degrees. Short straight dislocations array on the (001) plane were observed in the 45 degrees-orientated specimen. Grain rotation via grain boundary sliding and dislocation-mediated deformation were found to occur when the micro-sized magnets were deformed above 1000 degrees C.
Article
Nanoscience & Nanotechnology
Yao Lu, Kai Zhang, Bingbing Zhao, Xianping Dong, Feng Sun, Baoxue Zhou, Yunqian Zhen, Lanting Zhang
Summary: Al0.3CoCrFeNiTix (x = 0.025, 0.075, 0.15) high-entropy alloys (HEAs) were studied to investigate the effects of Ti addition and aging temperature on the mechanical properties. The alloy aged at 700 degrees C with x = 0.15 showed the highest ultimate tensile strength (UTS) and fracture elongation both at room temperature and 700 degrees C. The outstanding balanced mechanical properties of the alloy are attributed to the uniformly distributed L1(2) and B2 particles, which are promoted by Ti.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2023)
Article
Nanoscience & Nanotechnology
Ze Liu, Cai Chen, Yuanxun Zhou, Lanting Zhang, Hong Wang
Summary: Many studies have used machine learning to predict the glass-forming range of metallic glasses. However, the imbalanced and clustered datasets used for training the model make it difficult for the model to extrapolate. In this work, the generalization deficiency of the machine learning model was addressed by combining high-throughput experimentation and machine learning modeling, highlighting the importance of comprehensive data. Training the models with comprehensive data distribution over the composition space, it was found that data imbalance can lead to a skewed model and balanced data is crucial for the model's performance. An element-wise machine learning strategy was demonstrated to accelerate the identification of the glass-forming range.
SCRIPTA MATERIALIA
(2023)
Article
Materials Science, Multidisciplinary
Biao Wu, Haihui Zhang, Yuanxun Zhou, Lanting Zhang, Hong Wang
Summary: In this study, we propose an approach to determine the phase boundary and its uncertainty in a phase-composition map based on high-throughput experimentation. The approach combines Bayesian logistics regression with domain knowledge of phase diagrams and models both linear and nonlinear phase boundaries. The effectiveness of the approach is demonstrated using experimental data, and the uncertainty can be further reduced by incorporating data from subbinary systems.
PHYSICAL REVIEW MATERIALS
(2023)
Article
Materials Science, Multidisciplinary
Haihui Zhang, Biao Wu, Lanting Zhang, Hong Wang
Summary: Thermodynamic modelling and quantification of uncertainty are crucial for multicomponent alloy design. In this study, the Ag-Cu, Ag-Co, and Co-Cu binary systems were assessed and used to model the Ag-Cu-Co ternary system. The calculated phase diagrams agreed well with experimental results, and the reliability of the models was validated. The Phase Diagram Uncertainty Quantification tool provided confidence measures in the design of solder alloys.
MATERIALS CHEMISTRY AND PHYSICS
(2023)
Article
Chemistry, Physical
Jie Chen, Jian Liu, Minjuan Zhang, Zhanji Dong, Zhongjie Peng, Xinyi Ji, Mei Liu, Lanting Zhang, Anqi Zhang, Hong Zhu
Summary: Designing Nd-Fe-B-based permanent magnets with high temperature stability is crucial for their use in traction motors. Conventionally, heavy rare-earth elements are used for achieving high temperature stability, but at a higher cost. This study demonstrates the utilization of an adaptive learning framework to optimize the composition of Nd-Fe-B-based magnets with lower-cost elements and improve the performance-cost ratio. The framework efficiently screens novel compositions and guides the experimental design, resulting in significant improvements in the performance-cost ratio.
JOURNAL OF MATERIALS CHEMISTRY A
(2023)
Article
Nanoscience & Nanotechnology
Ze Liu, Cai Chen, Yuanxun Zhou, Lanting Zhang, Hong Wang
Summary: This study attempts to address the gap in cooling rates between thin film deposition and bulk metallic glass (BMG) casting by correlating the glass-forming range (GFR) determined from combinatorial materials chips (CMCs) with the glass-forming ability (GFA) of BMG. The results show that the full-width at half maximum (FWHM) of the first sharp diffraction peak (FSDP) is a good indicator of BMG GFA, and strong positive correlations between FWHM and the critical casting diameter (Dmax) are observed in various BMG systems. Furthermore, the Pearson correlation coefficients suggest possible similarities in the GFA natures of certain BMG pairs.
SCRIPTA MATERIALIA
(2024)