Journal
CHEMICAL COMMUNICATIONS
Volume 51, Issue 64, Pages 12819-12822Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc04300j
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Funding
- Natural Science Foundation of China [21172060, 21472039, 21402046]
- Specialized Research Fund for the Doctoral Program of Higher Education [20120161110041]
- Hunan Provincial Natural Science Foundation of China [13JJ2018]
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We here describe a new palladium-catalyzed oxidative 6-exo-trig cyclization of 1,6-enynes at room temperature using tBuONO as an oxidant for the synthesis of 3-bicyclo[4.1.0]heptan-5-ones. This cascade strategy involves the hydration, cyclization and cyclopropanation sequence, and represents a new transition-metal-catalyzed oxidative cyclization of 1,6-enynes in a 6-exo-trig fashion.
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