4.5 Article

Synthesis of silicate-1 monolith and its catalytic application

Journal

JOURNAL OF POROUS MATERIALS
Volume 24, Issue 4, Pages 881-886

Publisher

SPRINGER
DOI: 10.1007/s10934-016-0327-4

Keywords

Silicate-1 monolith; TiO2-loaded silicate-1 monolith; Catalytic activity

Funding

  1. Scientific Technological Innovation Platform of Fujian Province [2006L2003]

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Silicate-1 monolith was facilely synthesized in the precursor solution by combining sol-gel method and hydrothermal method. Characterization by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy and transmission electron microscope revealed that silicate-1 particles were formed by transforming amorphous SiO2 into MFI-type structure and inlayed into the three-dimensional network of silica to form the monolith. Then, silicate-1 monolith was used as support to load TiO2 by dip-coating method. TiO2 nanoparticles were well dispersed in silicate-1 monolith. The photocatalytic properties of all samples were evaluated based on the degradation efficiency of Rhodamine B. And a scheme regarding photodegradation enhancement induced by dye enrichments has been proposed to illustrate the adsorption-photodegradation process.

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