Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 3, Pages 831-841Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b02302
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Funding
- Department of Science and Technology (DST), Government of India [SR/S2/RJN-97/2012]
- University Grants Commission (UGC)
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We report here a practical method for the ortho C-H hydroxylation of benzamides with inexpensive copper(II) acetate monohydrate and a pyridine ligand. An intra- and intermolecular ligand combination was explored to achieve regio-and chemoselective hydroxylation. Interestingly, typical regiochemical scrambling associated with the C-H activation was further resolved by introducing a ligand-directed ortho hydroxylation of haloarenes and aryl methyl ethers.
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