Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 19, Pages 9350-9355Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.6b01988
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Funding
- NSFC [21232004, 21272095, 21472071]
- PAPD of Jiangsu Higher Education Institutions
- Outstanding Youth Fund of JSNU [YQ2015003]
- NSF of Jiangsu Province [BK20151163]
- Qing Lan Project
- NSF of Jiangsu Education Committee [15KJB150006]
- Graduate Education Innovation Project of Jiangsu Province [KYZZ15-0385]
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A new DDQ-mediated three-component dioxygenation of alkenes has been established, providing a direct and metal-free access toward densely functionalized 4,5-dichloro-3-hydroxyphthalonitrile derivatives with generally good to excellent yields under mild conditions. During this process, DDQ plays dual roles as both a dehydrogenation reagent and a coupling partner, enabling oxidative coupling to form two C-O functionalities in a highly atom-economy fashion.
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