Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 9, Pages 3860-3867Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.6b00522
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- Natural Sciences and Engineering Research Council (NSERC)
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A simple and regioselective synthesis of phenoxy esters and phenylthio esters is reported. The products are obtained by selective alkoxycarbonylation catalyzed by Pd-2(dba)(3), 1,4-bis(diphenylphisphino)butane (dppb), and syngas (CO/H-2) in chloroform/alcohol: This methodology affords bifunctional products in good yield with excellent n-selectivity and without the need to use additives.
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