Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 81, Issue 5, Pages 1905-1911Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b02726
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Funding
- National Research Foundation of Korea [NRF-2014R1A1A1A05003274, NRF-2014-011165, NRF-2012M3A7B4049657]
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An efficient visible-light photocatalysis-based one-pot amide synthesis method was developed; visible-light irradiation of a mixture of an aldehyde, tert-butyl hydrogen peroxide, and N-chlorosuccinimide using a Ru(bpy)(3)Cl-2 photocatalyst afforded an acid chloride, which subsequently reacted with amine to yield the corresponding amide. The reaction was used to synthesize modobemide and a D3 receptor intermediate.
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