4.7 Article

Microstructure evolution of graphene reinforced Cu/CeO2/Cr electrical contact materials under thermal deformation behavior

Journal

JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
Volume 18, Issue -, Pages 1412-1423

Publisher

ELSEVIER
DOI: 10.1016/j.jmrt.2022.03.038

Keywords

Graphene; Hot deformation; Flow stress; Electron backscattered diffraction (EBSD); Constitutive equations

Funding

  1. National Natural Science Foundation of China [52071134]
  2. Natural Science Foundation of Henan Province [202300410144]
  3. Program for Innovative Research Team in University of Henan Province [22IRTSTHN001]
  4. China Postdoctoral Science Foundation [2021T140779]
  5. Outstanding Talents Innovation Fund of Henan Province [ZYQR201912164]
  6. Scientific Research and Development Special Project of Henan Academy of Sciences [220910009]

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This study investigates the effect of graphene on the thermal deformation of Cu/CeO2/Cr and GO-Cu/CeO2/Cr composites. Experimental results and microstructure analysis reveal that graphene contributes to dispersion strengthening, twin strengthening, and grain refinement during thermal deformation, while inhibiting dynamic recrystallization. Additionally, increasing the deformation temperature strengthens the texture orientation, resulting in GO-Cu/CeO2/Cr composites with remarkable dynamic recovery characteristics and high-temperature properties.
The effect of graphene on the thermal deformation of Cu/CeO2/Cr and GO-Cu/CeO2/Cr composites was studied. The isothermal compression test was carried out with Gleeble-1500D thermomechanical simulation device in the range of 600-900 degrees C and strain rate of 0.001-1 s(-1). The microstructure after deformation was characterized and analyzed by optical microscope, scanning electron microscope (SEM), transmission electron microscope (TEM) and electron backscatter diffraction (EBSD). The interaction of work hardening, dynamic recovery and dynamic recrystallization was described. The constitutive equation was successfully established. The results show that Cr particles are extruded into strips, and nano CeO2 particles nail dislocations, which inhibit dynamic recovery and dynamic recrystallization. Dispersion strengthening, twin strengthening and grain refinement strengthening occur the thermal deformation of GO-Cu/CeO2/Cr composites, increase the flow stress and activation energy of the composites, and inhibit the dynamic recrystallization of the composites. When the hot deformation temperature increases, the texture orientation is strengthened. GO-Cu/CeO2/Cr composites have typical dynamic recovery characteristics and high temperature properties. (C) 2022 The Author(s). Published by Elsevier B.V

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