4.6 Article

Preparation and Electromagnetic Absorption Properties of Fe73.2Si16.2B6.6Nb3Cu1 Nanocrystalline Powder

Journal

MATERIALS
Volume 15, Issue 7, Pages -

Publisher

MDPI
DOI: 10.3390/ma15072558

Keywords

Fe-based nanocrystalline alloy; absorbing performance; soft-magnetic properties; electromagnetic shielding

Funding

  1. National Natural Science Foundation of China Project [51971049]
  2. Fundamental Research Funds for the Central Universities [DUT 19GF110]

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In order to decrease and control electromagnetic pollution, a nanocrystalline alloy ribbon with improved electromagnetic wave absorption properties was prepared and studied in this paper. The effects of ball milling time on the soft magnetic properties, microstructure, morphology, and electromagnetic wave absorption properties of the alloy powder were investigated. The results showed that the alloy powder obtained after 12 hours of ball milling had the best electromagnetic absorption performance.
In order to decrease and control electromagnetic pollution, absorbing materials with better electromagnetic wave absorption properties should be developed. In this paper, a nanocrystalline alloy ribbon with the composition of Fe73.2Si16.2B6.6Nb3Cu1 was designed and prepared. Nanocrystalline alloy powder was obtained by high-energy ball milling treatment. The effects of ball milling time on the soft magnetic properties, microstructure, morphology, and electromagnetic wave absorption properties of alloy powder were investigated. The results showed that, as time increased, alpha-(Fe, Si) gradually transformed into the amorphous phase, and the maximum saturation magnetization (M-s) reached 135.25 emu/g. The nanocrystalline alloy powder was flakelike, and the minimum average particle size of the powder reached 6.87 mu m. The alloy powder obtained by ball milling for 12 h had the best electromagnetic absorption performance, and the minimum reflection loss RLmin at the frequency of 6.52 GHz reached -46.15 dB (matched thickness was 3.5 mm). As time increased, the best matched frequency moved to the high-frequency direction, and the best matched thickness decreased, while the maximum effective absorption bandwidth Delta f(RL)(<-10 dB) was 7.22 GHz (10.78-18 GHz).

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