4.5 Article

Microwave foaming of carbon dioxide saturated poly lactic acid

Journal

POLYMER ENGINEERING AND SCIENCE
Volume 62, Issue 3, Pages 929-938

Publisher

WILEY
DOI: 10.1002/pen.25897

Keywords

3D printing; microwave; PLA; polymer foams; solid-state foaming

Funding

  1. Earl W. & Hildagunda A. Brinkman Private Charitable Foundation

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This study presents a solvent-free approach for the fabrication of microcellular poly lactic acid foams using additive manufacturing and microwave foaming. The results show that microwave foaming can generate foams with small pore size and high porosity. These foams fabricated through this approach have potential applications in the biomedical field.
Micro cellular polymer foams find numerous applications such as in filtration, tissue scaffolds, insulation, and catalyst carriers. This study reports on a solvent free approach to fabricate microcellular poly lactic acid foams through a combination of additive manufacturing and microwave foaming. This approach provides the capability to foam polymers in a repeatable and controllable manner with minimal human intervention. Initially, samples are 3D printed, followed by gas saturation, and microwave foaming. The effect of microwave foaming parameters, namely power, temperature and time on the pore morphology was analyzed using a complete parametric study. The results show that microwave foaming can successfully generate porous structure with power and temperature being the main factors affecting the pore morphology. A combination of midrange power and high temperature results in foams with desired properties of small pore size and high porosity. The resulting foams have pore size as small as 120 mu m with porosity of 78%. These foams fabricated using a solvent free approach find applications in biomedical field as three dimensional tissue scaffolds for drug testing and bio-artificial organ development.

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