Journal
GREEN CHEMISTRY
Volume 18, Issue 2, Pages 423-426Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5gc01505g
Keywords
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Funding
- Russian Science Foundation [15-13-10033]
- BRNS-DAE [37(2)/14/35/2014-BRNS/563]
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An efficient solvent-free procedure for the synthesis of pillar[6]-arenes has been developed. The procedure involves the solid-state condensation of finely milled 1,4-dialkoxybenzene and paraformaldehyde by grinding in the presence of a catalytic amount of H2SO4. The use of organic solvents for the extraction of products has also been avoided. Operational simplicity, compatibility with various 1,4-dialkoxybenzenes, non-chromatographic purification technique, high yields and mild reaction conditions are the notable advantages of this procedure. A large scale reaction demonstrated the practical applicability of this methodology.
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