Article
Materials Science, Multidisciplinary
M. Paghandeh, A. Zarei-Hanzaki, H. R. Abedi, Y. Vahidshad
Summary: The study investigates the strain accommodation mechanism of Ti-6Al-4V alloy with different initial microstructures under warm temperature deformation regime. Tensile tests were conducted at various temperatures, revealing different material behaviors and strain accommodation mechanisms in equiaxed alpha+beta, lamellar alpha+beta, dual phase alpha+alpha, and fully alpha martensite microstructures. The results provide insights into the relationship between microstructure, strain accommodation capability, and tensile formability.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2021)
Article
Materials Science, Multidisciplinary
O. Dumas, L. Malet, P. Kwasniak, F. Prima, S. Godet
Summary: The present study provides a detailed analysis of the microstructural characteristics of the Ti-4.5Al-2.5Fe-0.25Si alloy and its deformation mechanisms. The alloy exhibits remarkable work-hardening capabilities when the microstructural features are optimized. The Fe-enriched martensite induces reorientation through the motion of intervariant boundaries and the creation and growth of alpha' twins, contributing to the material's superior mechanical properties.
Article
Engineering, Manufacturing
Dylan Agius, Chris Wallbrink, Kyriakos Kourousis
Summary: The design freedom provided by Additive Manufacture (AM) technologies is driving innovation in new directions, but also creating challenges in material characterisation. This paper proposes a model that combines anisotropic yield function with nonlinear multicomponent kinematic hardening rule to accurately simulate the anisotropic behavior of materials like Ti-6Al-4V alloy. The model's performance was evaluated through simulations and showed good agreement with experimental data, demonstrating its efficiency in modeling cyclic stress-strain evolution in different build orientations.
ADDITIVE MANUFACTURING
(2021)
Article
Materials Science, Multidisciplinary
Aysun Ayday, Neslihan Ozsoy, Tuba Yener
Summary: In this study, the effects of electrolytic plasma treatment (EPT) on the hardness distribution, wear resistance, and surface morphologies of Ti-6Al-4V alloy at different thermal cycles were investigated. The results showed that the microstructure of the alloy could be controlled by adjusting the heat temperature and modification times of the thermal cycles during EPT processing. The hardness of the alloy was increased after the modification and the wear rate and coefficient of friction were examined through wear tests.
ADVANCED ENGINEERING MATERIALS
(2023)
Article
Chemistry, Physical
Zhuohan Cao, Qian Liu, Qianchu Liu, Xiaobo Yu, Jamie J. Kruzic, Xiaopeng Li
Summary: This study develops a machine learning-based approach using image data to predict and reconstruct the microstructural features of LPBF fabricated Ti-6Al-4V alloy. The results show that the proposed method can accurately predict the microstructural features under different process parameters, offering potential applications in process optimization and material design in additive manufacturing.
NPJ COMPUTATIONAL MATERIALS
(2023)
Article
Materials Science, Multidisciplinary
In-Su Kim, Jeong Mok Oh, Sang Won Lee, Jong-Taek Yeom, Jae-Keun Hong, Chan Hee Park, Taekyung Lee
Summary: This study investigated the effects of processing variables on the globularization of AM-processed Ti-6Al-4V alloy, revealing that a combination of solution treatment, low-temperature forging, and subsequent annealing significantly accelerates the process by reducing the path for boundary splitting in fine martensitic laths induced via solution treatment.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2021)
Article
Chemistry, Physical
Xudong Yan, Xiaofeng Xu, Yang Zhao, Yachong Zhou, Lai Wei, Zhicheng Wu, Yongqiang Yu, Chao Wu
Summary: Biomedical Ti-6Al-4 V-5.6Cu alloys with low elastic modulus, excellent work hardening, and outstanding corrosion resistance were achieved by manipulating the fractions of martensite phases made up of alpha '' and alpha '. The presence of alpha '' phase caused the low modulus, great work hardening, and high elongation. The optimized Ti-6Al-4 V-5.6Cu alloy exhibited strong potential for development as a biomedical implant material due to its combination of low elastic modulus (55 GPa), high YS/E ratio (10.25), excellent work hardening performance (Delta sigma = 848 MPa), and superior corrosion resistance.
JOURNAL OF ALLOYS AND COMPOUNDS
(2023)
Article
Materials Science, Coatings & Films
Yichen Meng, Matteo Villa, Kristian Dahl, Bo Wang, Michel Drouet, Jean-Baptiste Dubois, Marcel A. J. Somers, Thomas L. Christiansen
Summary: This study investigated the surface hardening and heat treatment response of Ti-6Al-4V grades G5 and G23 under different temperature and gaseous conditions. Various surface treatments were applied, resulting in different hardness values and structure formations. The diversity of treatments in this work represents the potential of gaseous and plasma-based thermochemical methods for surface engineering of titanium alloys.
SURFACE & COATINGS TECHNOLOGY
(2021)
Article
Chemistry, Physical
Xuefeng Zhou, Yulin Li, Ziru Han, Zilin Liu, Kaiwen Liu, Yiyou Tu, Feng Fang, Jianqing Jiang
Summary: A novel pathway for improving the work hardening capacity of Ti-6Al-4V alloy via simple solution in the virgin lower alpha + beta regime is proposed. Elemental partitioning and depletion of beta-stabilizers occur between alpha and beta phases as the solution temperature rises, resulting in the creation of metastable beta phases that transform into alpha '' martensite during mechanical straining. The stress-induced beta(m) -> alpha'' martensite transformation induces three-staged strain hardening and the desired transformation-induced plasticity effect, providing the alloy with a high strain hardening rate and good combinations of strength and ductility.
JOURNAL OF ALLOYS AND COMPOUNDS
(2023)
Article
Chemistry, Physical
K. Yang, X. Yang, Z. L. Zhang, T. T. Zhu, J. Li, X. S. Xiao, Y. X. Liang, B. Jian, C. Li, S. N. Luo
Summary: The spall damage of Ti-6Al-4V alloy fabricated via laser powder bed fusion (LPBF) was investigated through plate impact in the build direction (BD) and the transverse direction (TD), focusing on its mechanisms and microstructure effects. Comparative analysis was performed on conventionally hot-rolled Ti-6Al-4V alloys processed with annealing and quenching. Results showed that the spall strength and Hugoniot elastic limit (HEL) of LPBF-fabricated samples were higher in the TD loading than in the BD loading. The LPBF-fabricated alloy exhibited a lower HEL but similar spall strength compared to conventionally fabricated alloys. The anisotropy in mechanical properties and damage was attributed to columnar prior beta grains, morphological, and crystallographic texture of martensite laths.
JOURNAL OF ALLOYS AND COMPOUNDS
(2023)
Article
Materials Science, Multidisciplinary
Bo Yin, Jin Huang, Wei Xie, Jiale Wang, Shanshan Xu, Zhenhua Li
Summary: The addition of CaF2 during WAAM enhances the microstructure of titanium alloys, resulting in a high strength-ductility combination and improved mechanical properties.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2023)
Article
Materials Science, Multidisciplinary
Yifei Luo, Yuehuang Xie, Zhen Zhang, Jiamiao Liang, Deliang Zhang
Summary: A Ti-6Al-4V alloy with a dual harmonic structure was successfully fabricated by controlling grain sizes and element contents. This structure helps reduce mechanical mismatch and enhances strength and ductility.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2023)
Article
Materials Science, Multidisciplinary
Weidong Huang, Dongdong He, Hui Wang, Shuaishuai Qin, Lu Wang, Xiaopeng Xu
Summary: In this study, Ti-6Al-4V samples were fabricated by selective laser melting, and the effects of single and double annealing on the microstructure and mechanical properties anisotropy were investigated. The results showed that the annealing temperature had a significant influence on the morphology and structure of the samples, and the anisotropy could be reduced by both annealing methods.
Article
Nanoscience & Nanotechnology
Haiyang Fan, Chengcheng Wang, Yujia Tian, Kun Zhou, Shoufeng Yang
Summary: This study investigated the feasibility of using L-PBF to fabricate two Ti-6Al-4V-based bimetals, Ti-6Al-4V/γ-TiAl and Ti-6Al-4V/Ti-6242, which may have great potential for the future manufacturing of aerospace components. The bimetal Ti-6Al-4V/γ-TiAl was unsuccessfully built due to the intrinsic cold cracking of γ-TiAl processed by L-PBF. In comparison, the bimetal Ti-6Al-4V/Ti-6242 was successfully manufactured by L-PBF with a solid and defect-free interface.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2023)
Article
Mechanics
Xue Yang, Chenlin Liu, Yi Ding, Haodong Li, Yazhou Guo, Yulong Li
Summary: The paper investigates the dynamic plastic behavior of Ti-6Al-4V titanium alloy under complex loading conditions at high strain rates. By proposing a dynamic asymmetry yield criterion and loading surface, considering the coupling effects of strain rate and stress state, the reliability and accuracy of these models are validated. The study also reveals the non-uniformity in the initial yield surface and the expansion of loading surfaces under different stress states at high strain rates.
INTERNATIONAL JOURNAL OF SOLIDS AND STRUCTURES
(2023)
Article
Chemistry, Multidisciplinary
Fan Sun, Laurence Jordan, Valerie Albin, Virginie Lair, Armelle Ringuede, Frederic Prima
Article
Materials Science, Multidisciplinary
Kan Ma, Brigitte Decamps, Anna Fraczkiewicz, Frederic Prima, Marie Loyer-Prost
MATERIALS RESEARCH LETTERS
(2020)
Article
Materials Science, Multidisciplinary
Jinyong Zhang, Yangyang Fu, Yijin Wu, Bingnan Qian, Zheng Chen, Akihisa Inoue, Yuan Wu, Yang Yang, Fan Sun, Ju Li, Frederic Prima
MATERIALS RESEARCH LETTERS
(2020)
Article
Materials Science, Multidisciplinary
Ivan Guillot, Muriel Tyrman, Loic Perriere, Jean-Philippe P. Couzinie, Lola Lilensten, Frederic Prima, Guy Dirras
FRONTIERS IN MATERIALS
(2020)
Article
Materials Science, Multidisciplinary
Bingnan Qian, Jinyong Zhang, Yangyang Fu, Fan Sun, Yuan Wu, Jun Cheng, Philippe Vermaut, Frederic Prima
Summary: A new family of TRIP/TWIP Ti-alloys was developed to overcome the strength-ductility trade-off, with the dominant deformation mode transitioning from TRIP to TWIP with increasing Zr content. Different Ti-Mo-Zr alloys exhibit distinct plasticity characteristics, with high Zr content alloys demonstrating improved yield stress resistance.
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
(2021)
Article
Materials Science, Multidisciplinary
Yolaine Danard, Fan Sun, Thierry Gloriant, Immanuel Freiherr Von Thungen, Michael Piellard, Frederic Prima
FRONTIERS IN MATERIALS
(2020)
Article
Materials Science, Multidisciplinary
Chloe Varenne, Frederic Prima, Cedrik Brozek, Julie Bourgon, Jacques Besson, Anne-Francoise Gourgues-Lorenzon
Summary: Titanium alloys with twinning- and transformation-induced plasticity effects exhibit high impact toughness. Research on the Ti-Cr-Sn alloy revealed that twins play a major role in the fracture process, significantly affecting its impact toughness.
JOURNAL OF MATERIALS SCIENCE
(2021)
Article
Materials Science, Biomaterials
Fan Sun, Laurence Jordan, Alexandre da Silva, Frantz Martin, Frederic Prima
Summary: The study investigates the impact of hydrogen on the mechanical properties of NiTi, finding that 8 wppm hydrogen has minimal effect while 40 wppm hydrogen significantly decreases martensitic transformation temperature and macroscopic ductility. Through techniques like electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM), the effects of hydrogen on NiTi are studied at different length scales.
MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS
(2021)
Article
Materials Science, Multidisciplinary
Benoit Fer, David Tingaud, Azziz Hocini, Yulin Hao, Eric Leroy, Frederic Prima, Guy Dirras
Letter
Materials Science, Multidisciplinary
Jinyong Zhang, Bingnan Qian, Yijin Wu, Yu Wang, Jun Cheng, Zheng Chen, Jinshan Li, Fan Sun, Frederic Prima
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
(2021)
Article
Materials Science, Multidisciplinary
Stephanie Delannoy, Sarah Baiz, Pascal Laheurte, Laurence Jordan, Frederic Prima
Summary: The study aimed to develop a thermo-mechanical strategy to create a radial elasticity gradient in a beta metastable Ti-Nb-Zr alloy, and to lower the elastic modulus of the alloy through mechanical deformation. Experimental results showed that shot-peening was an efficient way to induce surface martensitic transformation and create an elasticity gradient in beta metastable titanium alloys, potentially suitable for producing dental implants with mechanically enhanced biocompatibility.
FRONTIERS IN MATERIALS
(2021)
Article
Materials Science, Multidisciplinary
Kan Ma, Brigitte Decamps, Anna Fraczkiewicz, Thomas Jourdan, Frederic Prima, Marie Loyer-Prost
Summary: The study shows: (i) significant influence of specimen thickness on microstructural evolution and irradiated microstructure with a critical thickness depending on temperature; (ii) accurate prediction of an adequate irradiation thickness using a vacancy concentration calculation model; (iii) impact of free surfaces on the fine distribution of loop Burgers vectors.
Article
Materials Science, Multidisciplinary
L. Lilensten, Y. Danard, R. Poulain, R. Guillou, J. M. Joubert, L. Perriere, P. Vermaut, D. Thiaudiere, F. Prima
Article
Materials Science, Multidisciplinary
D. M. Gordin, F. Sun, D. Laille, F. Prima, T. Gloriant
Article
Materials Science, Multidisciplinary
Y. Liu, K. Zweiacker, C. Liu, J. T. McKeown, J. M. K. Wiezorek
Summary: The evolution of rapid solidification microstructure and solidification interface velocity of hypereutectic Al-20at.%Cu alloy after laser melting has been studied experimentally. It was found that the formation of microstructure was dominated by eutectic, alpha-cell, and banded morphology grains, and the growth modes changed with increasing interface velocity.
Article
Materials Science, Multidisciplinary
Bharat Gwalani, Julian Escobar, Miao Song, Jonova Thomas, Joshua Silverstein, Andrew Chihpin Chuang, Dileep Singh, Michael P. Brady, Yukinori Yamamoto, Thomas R. Watkins, Arun Devaraj
Summary: Castable alumina forming austenitic alloys exhibit superior creep life and oxidation resistance at high temperatures. This study reveals the mechanism behind the enhanced creep performance of these alloys by suppressing primary carbide formation and offers a promising alloy design strategy for high-temperature applications.
Article
Materials Science, Multidisciplinary
Jian Song, Qi Zhang, Songsong Yao, Kunming Yang, Houyu Ma, Jiamiao Ni, Boan Zhong, Yue Liu, Jian Wang, Tongxiang Fan
Summary: Recent studies have shown that achieving an atomically flat surface for metals can greatly improve their oxidation resistance and enhance their electronic-optical applications. Researchers have explored the use of graphene as a covering layer to achieve atomically flat surfaces. They found that high-temperature deposited graphene on copper surfaces formed mono-atomic steps, while annealed copper and transferred graphene on copper interfaces formed multi-atomic steps.
Article
Materials Science, Multidisciplinary
Jennifer A. Glerum, Jon-Erik Mogonye, David C. Dunand
Summary: Elemental powders of Al, Ti, Sc, and Zr are blended and processed via laser powder-bed fusion to create binary and ternary alloys. The microstructural analysis and mechanical testing show that the addition of Ti results in the formation of primary precipitates, while the addition of Sc and Zr leads to the formation of fine grain bands. The Al-0.25Ti-0.25Zr alloy exhibits comparable strain rates to Al-0.5Zr at low stresses, but significantly higher strain rates at higher stresses during compressive creep testing. Finite element modeling suggests that the connectivity of coarse and fine grain regions is a critical factor affecting the creep resistance of the alloys.
Article
Materials Science, Multidisciplinary
P. Jannotti, B. C. Hornbuckle, J. T. Lloyd, N. Lorenzo, M. Aniska, T. L. Luckenbaugh, A. J. Roberts, A. Giri, K. A. Darling
Summary: This work characterizes the thermo-mechanical behavior of bulk nanocrystalline Cu-Ta alloys under extreme conditions. The experiments reveal that the alloys exhibit unique mechanical properties, behaving differently from conventional nanocrystalline Cu. They do not undergo grain coarsening during extrusion and exhibit behavior similar to coarse-grained Cu.
Article
Materials Science, Multidisciplinary
Yiqing Wei, Jingwei Li, Daliang Zhang, Bin Zhang, Zizhen Zhou, Guang Han, Guoyu Wang, Carmelo Prestipino, Pierric Lemoine, Emmanuel Guilmeau, Xu Lu, Xiaoyuan Zhou
Summary: This study proposes a new strategy to modify microstructure by phase regulation, which can simultaneously enhance carrier mobility and reduce lattice thermal conductivity. The addition of Cu in layered SnSe2 induces a phase transition that leads to increased grain size and reduced stacking fault density, resulting in improved carrier mobility and lower lattice thermal conductivity.
Article
Materials Science, Multidisciplinary
Jia Chen, Zhengyu Zhang, Eitan Hershkovitz, Jonathan Poplawsky, Raja Shekar Bhupal Dandu, Chang-Yu Hung, Wenbo Wang, Yi Yao, Lin Li, Hongliang Xin, Honggyu Kim, Wenjun Cai
Summary: In this study, the structural origin of the pH-dependent repassivation mechanisms in multi-principal element alloys (MPEA) was investigated using surface characterization and computational simulations. It was found that selective oxidation in acidic to neutral solutions leads to enhanced nickel enrichment on the surface, resulting in reduced repassivation capability and corrosion resistance.
Article
Materials Science, Multidisciplinary
X. Y. Xu, C. P. Huang, H. Y. Wang, Y. Z. Li, M. X. Huang
Summary: The limited slip systems of magnesium (Mg) and its alloys hinder their wide applications. By conducting tensile straining experiments, researchers discovered a rate-dependent transition in the dislocation mechanisms of Mg alloys. At high strain rates, glissile dislocations dominate, while easy-glide dislocations dominate at low strain rates. Abundant glissile dislocations do not necessarily improve ductility.
Article
Materials Science, Multidisciplinary
M. S. Szczerba, M. J. Szczerba
Summary: Inverse temperature dependences of the detwinning stress were observed in face-centered cubic deformation twins in Cu-8at.%Al alloy. The detwinning stress increased with temperature when the pi detwinning mode was involved, but decreased when the pi/3 mode was involved. The dual effect of temperature on the detwinning stress was due to the reduction of internal stresses pre-existing within the deformation twins. The complete reduction of internal stresses at about 530 degrees C led to the equivalence of the critical stresses of different detwinning modes and a decrease in the yield stress anisotropy of the twin/matrix structure.
Article
Materials Science, Multidisciplinary
Taowen Dong, Tingting Qin, Wei Zhang, Yaowen Zhang, Zhuoran Feng, Yuxiang Gao, Zhongyu Pan, Zixiang Xia, Yan Wang, Chunming Yang, Peng Wang, Weitao Zheng
Summary: The interaction between the electrode and the electric double layer (EDL) significantly influences the energy storage mechanism. By studying the popular alpha-Fe2O3 electrode and the EDL interaction, we find that the energy storage mechanism of the electrode can be controlled by modulating the EDL.
Article
Materials Science, Multidisciplinary
Matthew R. Barnett, Jun Wang, Sitarama R. Kada, Alban de Vaucorbeil, Andrew Stevenson, Marc Fivel, Peter A. Lynch
Summary: The elastic-plastic transition in magnesium alloy Mg-4.5Zn exhibits bursts of deformation, which are characterized by sudden changes in grain orientation. These bursts occur in a coordinated manner among nearby grains, with the highest burst rate observed at the onset of full plasticity. The most significant burst events are associated with twinning, supported by the observation of twinned structures using electron microscopy. The bursts are often preceded and followed by a stasis in peak movement, indicating a certain "birth size" for twins upon formation and subsequent growth at a later stage.
Article
Materials Science, Multidisciplinary
Vaidehi Menon, Sambit Das, Vikram Gavini, Liang Qi
Summary: Understanding solute segregation thermodynamics is crucial for investigating grain boundary properties. The spectral approach and thermodynamic integration methods can be used to predict solute segregation behavior at grain boundaries and compare with experimental observations, thus aiding in alloy design and performance control.
Article
Materials Science, Multidisciplinary
Feiyu Qin, Lei Hu, Yingcai Zhu, Yuki Sakai, Shogo Kawaguchi, Akihiko Machida, Tetsu Watanuki, Yue-Wen Fang, Jun Sun, Xiangdong Ding, Masaki Azuma
Summary: This study reports on the negative and zero thermal expansion properties of Cd2Re2O7 and Cd1.95Ni0.05Re2O7 materials, along with their ultra-low thermal conductivity. Through investigations of their structures and phonon calculations, the synergistic effect of local structure distortion and soft phonons is revealed as the key to achieving these distinctive properties.
Article
Materials Science, Multidisciplinary
Thomas Beerli, Christian C. Roth, Dirk Mohr
Summary: A novel testing system for miniature specimens is designed to characterize the plastic response of materials for which conventional full-size specimens cannot be extracted. The system has an automated operation process, which reduces the damage to specimens caused by manual handling and improves the stability of the test results. The experiments show that the miniature specimens extracted from stainless steel and aluminum have high reproducibility, and the results are consistent with those of conventional-sized specimens. A correction procedure is provided to consider the influence of surface roughness and heat-affected zone caused by wire EDM.
Article
Materials Science, Multidisciplinary
Rani Mary Joy, Paulius Pobedinskas, Nina Baule, Shengyuan Bai, Daen Jannis, Nicolas Gauquelin, Marie-Amandine Pinault-Thaury, Francois Jomard, Kamatchi Jothiramalingam Sankaran, Rozita Rouzbahani, Fernando Lloret, Derese Desta, Jan D'Haen, Johan Verbeeck, Michael Frank Becker, Ken Haenen
Summary: This study investigates the influence of film microstructure and composition on the Young's modulus and residual stress in nanocrystalline diamond thin films. The results provide insights into the mechanical properties and intrinsic stress sources of these films, and demonstrate the potential for producing high-quality nanocrystalline diamond films under certain conditions.