Journal
PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES
Volume 125, Issue -, Pages -Publisher
ELSEVIER
DOI: 10.1016/j.physe.2020.114381
Keywords
ZnO nanoparticles; Rietveld analysis; Willamson-Hall method (W-H) analysis; Optical properties
Funding
- Conacyt Catedra Programs [352-2018]
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This study investigated the structural, microstructural, and optical properties of Mg-doped ZnO nanoparticles prepared through thermal decomposition route. Rietveld analysis revealed a hexagonal wurtzite structure with changes in lattice parameters and bond length. SEM analysis showed morphological changes in the nanoparticles with different Mg doping concentrations, while UV-Visible spectroscopy and PL studies provided insights into the optical characteristics of the material.
The structural, microstructural, and optical properties of Mg-doped ZnO nanoparticles prepared via. thermal decomposition route. The Rietveld analysis was executed for prepared sample, which revealed that the hexagonal wurtzite structure for all samples along with changes in lattice parameters and bond length. The various relevant parameters, such as strain, stress, and energy density, are analyzed using different improved forms of W-H equations via. a complete Willamson-Hall (W-H) method. Scanning electron microscopy (SEM) analysis resultant that the synthesized nanoparticles (NP's) are nearly spherical for Zn1-xMgxO, up to x = 0.04, and transform into a rectangular shape for x = 0.10. UV-Visible spectroscopy revealed an observation of fundamental absorption peak around 375 nm, which further shifted towards the higher wavelength, recommended the blue shift in the bandgap energy. The photoluminescence (PL) studies show a green emission band at 550 nm, demonstrating the occurrence of oxygen vacancy defects in the lattice of ZnO.
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