Journal
DALTON TRANSACTIONS
Volume 45, Issue 21, Pages 8972-8983Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5dt04969e
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Funding
- Fundamental Research Funds for the Central Universities [lzujbky-2015-16]
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An efficient catalyst based on the cage-like mesoporous material SBA-16 as the support and Cu(I) as active sites has been successfully prepared. The catalyst demonstrated high catalytic activity (up to 88%) in the direct oxidative synthesis of alpha-ketoamides between acetophenone and piperidine, employing O-2 from open air as the oxidant without other additives. A heterogeneous catalyst was applied in this reaction for the first time, and the catalyst could be easily separated from the reaction system by filtration and reused several times without a significant loss of activity.
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