Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 85, Issue 21, Pages 13939-13950Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.0c01985
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Funding
- SERB, India [ECR/2016/000270]
- DST-INSPIRE [IFA 13-CH-90]
- IIT(ISM) Dhanbad
- DST-INSPIRE
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An organic dye-catalyzed visible light-promoted ketocarbonylation protocol of vinyl arenes has been disclosed with the help of alpha-bromocarbonyls where aerial oxygen played a role of an oxidant to install the keto-oxygen functionality. This unique process is compatible with both internal and terminal olefins and tolerates a diverse array of functional groups (ketone, ester, amide, diketones, ketoester, and malonate). This process is mild and environmentally friendly and deals with greener oxidants like oxygen, affording 1,4-ketocarbonyls as a value-added end product.
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