Journal
JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY
Volume 89, Issue -, Pages 368-374Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.jiec.2020.06.005
Keywords
Layered double hydroxide; Nanofiltration; Calcination; Surface free energy; Enhanced performance
Funding
- National Natural Science Foundation of China [21776003]
- Beijing Natural Science Foundation [2182004]
- Beijing Nova Program [Z181100006218079]
- Beijing Municipal Natural Science Foundation - Beijing Natural Science Foundation Committee
- Beijing Education Committee [KZ201910005001]
- Importation and Development of High-Caliber Talents Project of Beijing Municipal Institutions [CITTCD20170305, CITTCD201904014]
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Two-dimensional layered double hydroxides (LDH) as a membrane material has tremendous potential in the water treatment field. However, the stability and permeance of the LDH membrane should be further improved for the industrial application. In this study, the LDH separation layer was in situ grown on the tubular Al2O3 substrate. The obtained LDH composite membrane was then calcined to reduce the surface free energy and remove some interlayer anions. Therefore, the calcined LDH composite membrane exhibited enhanced stability and permeance for removing dye molecules from water. The permeance of the calcined LDH membrane reached 367 Lm(-2)h(-1)MPa(-1) and the rejection for Eriochrome black T was still above 99%. Moreover, the membrane can maintain the separation performance more than 110 h in the nanofiltration process. The morphologies and structures of the LDH membranes before and after calcination were also investigated. The results indicated that this facile method is effective to improve the separation performance of the LDH membrane. (C) 2020 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.
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