Journal
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
Volume 65, Issue 6, Pages 839-845Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023620060261
Keywords
cluster boron anions; nitrilium derivatives; complex compounds
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Funding
- Russian Scientific Foundation [18-13-00459]
- Russian Science Foundation [18-13-00459] Funding Source: Russian Science Foundation
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A two-stage method for the synthesis of a boron-containing complexone on the basis of aminomalonic acid was proposed. The products were studied by multinuclear NMR spectroscopy, IR absorption spectroscopy, and ESI mass spectrometry at all the stages of synthesis. The product (NBu4)[2-B10H9NHC(CH3)NHCH(COOEt)(2)] was structurally characterized by singe-crystal X-ray diffraction. The complexation reaction between the borylated derivative of aminomalonic acid and Hf(NEt2)(4)and Hf(OBu)(4)was studied.
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