4.3 Article

Hot deformation behaviour of bimodal sized Al2O3/Al nanocomposites fabricated by spark plasma sintering

Journal

JOURNAL OF MICROSCOPY
Volume 281, Issue 1, Pages 28-45

Publisher

WILEY
DOI: 10.1111/jmi.12947

Keywords

Bimodal reinforcement; constitutive modelling; hot forming; metal matrix nanocomposites (MMCs); spark plasma sintering (SPS)

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The deformation behavior and dynamic recrystallization behavior of bimodal sized Al2O3/Al nanocomposites were studied under hot compression tests, showing that bimodal sized Al(2)O(3) particles played a crucial role in the recrystallized microstructure. Moreover, the addition of bimodal sized Al(2)O(3) particles led to a significant increase in activation energy of plastic deformation, contributing to the enhanced resistance of the nanocomposite to hot deformation.
The deformation behaviour of bimodal sized Al2O3/Al nanocomposites were investigated by hot compression tests conducted in the temperature range 350-500 degrees C and strain rates of 0.001, 0.01 and 0.1 s(-1). The dynamic recrystallisation behaviour of the nanocomposites strongly depended on the forming parameters. The bimodal sized Al(2)O(3)particles played a crucial role in the recrystallised microstructure. The addition of bimodal sized Al(2)O(3)particles led to a significant increase of activation energy of plastic deformation, corroborating the enhanced resistance of the nanocomposite to hot deformation. This was also reflected by the increased compressive yield strength in the nanocomposite due to both dislocation strengthening caused by n-Al(2)O(3)and preventing the grain growth due to the presence of mu-Al(2)O(3)at grain boundaries. It was found that with the decrease ofZvalues, local strain induced by deformation was released and the grain size of aluminium matrix gradually increased, indicating that the main softening mechanism of the bimodal sized Al2O3/Al nanocomposites was dynamic recrystallisation (DRX). The lower theZvalue was, the easier the DRX occurred. The highly beneficial role of the bimodal sized Al(2)O(3)reinforcement in improving the high-temperature performance of aluminium matrix nanocomposite was discussed.

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