Journal
HOLZFORSCHUNG
Volume 74, Issue 12, Pages 1147-1155Publisher
WALTER DE GRUYTER GMBH
DOI: 10.1515/hf-2019-0287
Keywords
furfurylation; imaging FT-IR; nanoindentation; NMR; wood
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Funding
- National Natural Science Foundation of China [31800474, 31770600]
- National Key R&D Program of China [2017YFD0600803]
- State Special Research Fund of Forestry Public Welfare of China [201404510]
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The aim of this investigation was mainly to evaluate the multi-scale distribution of furfuryl alcohol (FA) resin in modified Chinese fir and poplar wood. C-13 CP/ MAS NMR, Scanning Electron Microscopy (SEM), Confocal Laser Scanning Microscopy (CLSM), Nanoindentation and Imaging Fourier transform infrared microscopy (Imaging FT-IR) were applied to describe the FA resin distribution in wood from bulk to cell wall scale. The results showed that FA resin were mainly located in the cell cavity of Chinese fir tracheids. For poplar, FA resin was mostly deposited in the cavity of fibers and ray cells, while little was found in the adjacent vessels. Lots of pits of wood cells were covered with FA resin which implied a higher risk of drying after wood furfurlation in practical production. Nanoindentation demonstrated that FA resin could easily infiltrate into the wood cell wall because both reduced modulus and hardness of the modified wood cell walls were significantly improved. This conclusion was further supported by the results of imaging FT-IR.
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