Journal
PROCESSES
Volume 8, Issue 6, Pages -Publisher
MDPI
DOI: 10.3390/pr8060647
Keywords
5-hydroxymethylfurfural; 2,5-diformylfuran; TiO2; electrochemical synthesis; pulse alternating current
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Funding
- RUSSIAN SCIENCE FOUNDATION [16-13-10444]
- Russian Science Foundation [16-13-10444, 19-13-13049] Funding Source: Russian Science Foundation
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TiO2 nanoparticles were prepared via an electrochemical method using pulse alternating current and applied in the photocatalytic oxidation of 5-hydroxymethylfurfural (HMF) to 2,5-diformylfuran (DFF). Its physicochemical properties were characterized by SEM, HRTEM, XRD, and BET methods. The effect of scavenger and UVA light intensity was studied. The results revealed that electrochemically synthesized TiO2 nanoparticles exhibit higher DFF selectivity in the presence of methanol (up to 33%) compared with commercial samples.
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