Journal
CHEMISTRY-A EUROPEAN JOURNAL
Volume 22, Issue 25, Pages 8462-8465Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201601145
Keywords
coordination chemistry; diffusion coefficients; molecular weights; NMR solvents; structure elucidation
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Funding
- DNRF [DNRF93]
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New external calibration curves (ECCs) for the estimation of aggregation states of small molecules in solution by DOSY NMR spectroscopy for a range of different common NMR solvents ([D-6]DMSO, C6D12, C6D6, CDCl3, and CD2Cl2) are introduced and applied. ECCs are of avail to estimate molecular weights (MWs) from diffusion coefficients of previously unknown aggregates. This enables a straightforward and elaborate examination of (de)aggregation phenomena in solution.
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