Journal
CHEMICAL COMMUNICATIONS
Volume 52, Issue 5, Pages 919-921Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5cc08486e
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Funding
- EPSRC [EP/L023652/1, EP/K038885/1, EP/H024107/1, EP/K023004/1, EP/K021966/1, EP/I033459/1, EP/J015156/1]
- EU project [318671 MICREAGENTS]
- University of Glasgow
- Engineering and Physical Sciences Research Council [EP/L023652/1, EP/I033459/1, EP/K023004/1, EP/H024107/1, EP/K021966/1, EP/K038885/1, EP/J015156/1] Funding Source: researchfish
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We report the formation of two polyoxotungstates of the general formula [M-6(PW6O26)(alpha-P2W15O56)(2)(H2O)(2)](23-) (M = Co-II or Mn-II), which contain {PW6} fragments generated from the [P2W15O56](12-) precursor, which demonstrates for the first time the transformation of a Dawson lacunae into a Keggin lacunary building block. Solution analysis of the clusters has been conducted via electrospray ionisation mass spectrometry.
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