Journal
ANALYTICAL SCIENCES
Volume 36, Issue 5, Pages 617-620Publisher
JAPAN SOC ANALYTICAL CHEMISTRY
DOI: 10.2116/analsci.19SBN02
Keywords
Chromium; soil extract; ion transfer device; GFAAS
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Funding
- Environment Research and Technology Development Fund of the Environmental Restoration and Conservation Agency of Japan [5RF-1602]
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Electrodialytic separation of Cr(VI) and Cr(III) followed by graphite furnace atomic absorption spectrometry for monitoring of soil extraction was studied. The sensitivity was improved by in-line purification of the solutions and bi-polar pulse cleaning. The detection limit for both Cr(VI) and Cr(III) was 0.01 mu g L-1. The system was successfully used to monitor the concentration change during soil extraction with dual solution line filtration. The results demonstrate the difference in concentration changes with the different sources of Cr(VI).
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