Article
Materials Science, Multidisciplinary
Kai Hu, Yanjin Guan, Jiqiang Zhai, Yi Li, Fengjiao Chen, Ya Liu, Jun Lin
Summary: Multi-pass friction stir processing (MFSP) is an effective method to enhance the mechanical properties, plasticity, and corrosion resistance of Mg-Li alloy. The tensile strength and microhardness of the treated plate have been improved, and the elongation increased by up to 109.2%.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2022)
Article
Chemistry, Physical
S. Aravind Krishna, N. Radhika, Bassiouny Saleh, S. Manivannan
Summary: In this study, CoCrFeCuTi High Entropy Alloys (HEA) powder was reinforced on an SS304 steel substrate using a Friction Stir Processing (FSP) approach to achieve grain size refinement and improvement in mechanical properties. The microstructural analysis showed better grain refinement and dispersion of HEA reinforcement in the processed substrate. The Vickers microhardness and tensile strength were improved and the FSP-processed substrate with HEA also exhibited better resistance to corrosion.
JOURNAL OF ALLOYS AND COMPOUNDS
(2023)
Article
Materials Science, Multidisciplinary
Luyao Jiang, Wen Jiang, Fei Guo, Weijiu Huang, Haipeng Dong, Hongjun Hu, Qingwei Dai
Summary: Friction stir processing was successfully conducted on ultra-light dual-phase LZ91 Mg-Li alloy, resulting in refined microstructure and mixed phase structure. The process parameters significantly influenced the material flow modes and led to phase refinement in the stir zone.
MATERIALS CHARACTERIZATION
(2021)
Article
Materials Science, Multidisciplinary
Mahya Elyasi, Ahmad Razaghian, Ali Moharami, Masoud Emamy
Summary: This study investigates the microstructure and tensile properties of Mg-0.5Zn-0.2Si-XZr (X: 0, 0.25, 0.5 wt.%) under different processing conditions. Micro addition of Zr element can reduce grain size, but it is affected by Si poisoning effect. Processing the Zr-free alloy can improve its microstructure and mechanical properties. Further improvement in microstructure and mechanical properties can be achieved by multiple-pass FSP treatment of Zr-modified alloys.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2022)
Article
Chemistry, Physical
Jinghua Zhang, Ruidong Fu, Yijun Li, Yu Lei, Liang Guo, Hongyan Lv, Jinxiu Yang
Summary: The strength and ductility of nitrogen-alloyed CoCrFeMnNi high-entropy alloys (HEAs) were synergistically enhanced by multi-pass friction stir processing (FSP), resulting in refinement of the processed zone and a decrease in average grain size (AGS) with each FSP pass. Nitrogen-alloyed CoCrFeMnNi HEAs also exhibited a higher fraction of low angle boundaries (LABs) after FSP. The interaction between nitrogen atoms and LABs during FSP was indirectly proved by comparing the microstructural thermal-stability between different HEAs groups.
JOURNAL OF ALLOYS AND COMPOUNDS
(2022)
Article
Materials Science, Multidisciplinary
Miao Wang, Xingwei Huang, Peng Xue, Shangquan Wu, Chuanyong Cui, Qingchuan Zhang
Summary: In this study, friction stir processing (FSP) was used to process a high-strength and high-melting-point Ni-Co based superalloy, achieving enhanced strength and ductility. The FSP samples exhibited significantly higher yield strength and ultimate tensile strength at both room temperature and 400 degrees C, demonstrating a synergy between strength and ductility. The mechanisms contributing to the improved mechanical properties, such as grain-boundary and nanotwin strengthening, were investigated and discussed.
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
(2022)
Article
Materials Science, Multidisciplinary
Sam Yaw Anaman, Solomon Ansah, Hoon-Hwe Cho, Min-Gu Jo, Jin-Yoo Suh, Minjung Kang, Jong-Sook Lee, Sung-Tae Hong, Heung Nam Han
Summary: The study investigated the electrochemical properties and microstructural evolution of FSPed HEA, and found that the formation of Cr2O3 passive layer enhanced the corrosion resistance of the alloy. Grain refinement in the stir zone facilitated the rapid formation of the passive layer, leading to better corrosion properties on the front surface. The micro-galvanic nature of HEA may contribute to the localized corrosion behavior observed.
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
(2021)
Article
Metallurgy & Metallurgical Engineering
Miao Wang, Xing-Wei Huang, Peng Xue, Chuan-Yong Cui, Qing-Chuan Zhang
Summary: Friction stir processing was applied to high-strength and high-melting-point Ni-Fe-based superalloy for the first time, resulting in negligible tool wear. Different rotation rates were found to impact microstructure and tensile properties, with continuous dynamic recrystallization identified as the grain refinement mechanism.
ACTA METALLURGICA SINICA-ENGLISH LETTERS
(2021)
Article
Materials Science, Multidisciplinary
William P. Bates, Vivek Patel, Harikrishna Rana, Joel Andersson, Jeroen De Backer, Mattias Igestrand, Livan Fratini
Summary: The present study aims to enhance the mechanical properties of hypereutectic aluminium-silicon castings by modifying the microstructure and reducing defects through friction stir processing (FSP). By altering the tool revolution and the number of FSP passes, the study identified the specimen with the highest number of passes to have the most uniform properties, resulting from reduced casting porosities and refined silicon particle distribution in the friction stir processed zone.
METALS AND MATERIALS INTERNATIONAL
(2023)
Review
Nanoscience & Nanotechnology
Hamed Mirzadeh
Summary: This overview article summarizes the high strain rate superplasticity achieved through friction stir processing (FSP), emphasizing the importance of microstructural characteristics for superplastic forming operations. It also discusses the effects of main processing parameters on heat input and grain size, as well as recent progress in the application of FSP for processing superplastic materials.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2021)
Article
Materials Science, Multidisciplinary
Lin Ma, Changzhuang Zhou, Yao Shi, Qinghe Cui, Shude Ji, Kang Yang
Summary: The experiments comparing conventional friction stir processing and ultrasonic-assisted friction stir processing showed that ultrasound can enhance grain refinement in the as-cast A356 aluminium alloy, particularly with relatively high processing heat-input. Ultrasonic vibration also positively impacted the hardness, tensile strength, and elongation of the alloy.
METALS AND MATERIALS INTERNATIONAL
(2021)
Article
Materials Science, Multidisciplinary
Vivek Patel, Wenya Li, Joel Andersson, Na Li
Summary: This study focuses on the refinement of microstructure and evaluation of corrosion behavior in thick AZ31B magnesium alloy using stationary shoulder friction stir processing (SSFSP). The results show that the use of stationary shoulder reduces heat input and temperature gradient in the stir zone, leading to improved corrosion resistance of the alloy.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2022)
Article
Metallurgy & Metallurgical Engineering
Mehrab Lotfpour, Changiz Dehghanian, Massoud Emamy, Ahmad Bahmani, Mehdi Malekan, Ahmad Saadati, Milad Taghizadeh, Mohammadreza Shokouhimehr
Summary: In this study, a new biodegradable Mg-Zn-Cu magnesium alloy was introduced for biological applications. Addition of 0.1wt.% Cu was found to enhance corrosion resistance, with extruded alloys displaying better corrosion resistance behavior compared to cast alloys. The Mg-2Zn-0.1Cu alloy was identified as a potential candidate for use as a biodegradable magnesium implant due to its improved tensile properties.
JOURNAL OF MAGNESIUM AND ALLOYS
(2021)
Article
Mechanics
M. V. N. V. Satyanarayana, Soumya Bathula, Adepu Kumar
Summary: Friction stir processing improves ductility and fatigue behavior of aluminum alloy, and external cooling can further reduce fatigue crack growth rate.
ENGINEERING FRACTURE MECHANICS
(2022)
Article
Materials Science, Multidisciplinary
Gh Asrari, M. H. Daneshifar, S. A. Hosseini, M. Alishahi
Summary: This study demonstrated the fabrication of an Al-Mg solid solution layer on a pure Al substrate using friction stir selective alloying, resulting in significantly increased hardness compared to the original sample.
Article
Materials Science, Multidisciplinary
Shebeer A. Rahim, T. T. Nikhil, M. A. Joseph, T. Hanas
Summary: The study investigated the use of calcium phosphate (CaP) coating on magnesium-calcium alloys in physiological environments to improve biomineralization and reduce degradation rates. The CaP coating was found to help control the reduction in mechanical properties of the alloys in physiological environments.
MATERIALS TECHNOLOGY
(2021)
Article
Metallurgy & Metallurgical Engineering
Shebeer A. Rahim, V. P. Muhammad Rabeeh, M. A. Joseph, T. Hanas
Summary: The surface modification of Mg-Ca alloy by acid pickling significantly improved biomineralization and developed in situ calcium phosphate coating. Treated samples showed reduced degradation rate in simulated body fluid (SBF) compared to untreated samples, suggesting acid pickling as an effective method to tailor the performance of Mg-Ca alloy in physiological environment.
JOURNAL OF MAGNESIUM AND ALLOYS
(2021)
Article
Materials Science, Composites
Shebeer A. Rahim, G. Unnikrishnan, M. A. Joseph, Mubarak Ali, Asif Afzal
Summary: The study found that the mechanical properties of NBR increase at a specific loading level of chitosan; a Chitosan Efficacy Index is proposed to evaluate the impact of chitosan on overall mechanical properties; morphological examinations, thermogravimetric analysis, and water absorption studies were conducted to complement the experimental results.
PLASTICS RUBBER AND COMPOSITES
(2022)
Review
Materials Science, Multidisciplinary
Shebeer A. Rahim, M. A. Joseph, T. S. Sampath Kumar, Hanas Hanas
Summary: This article reviews recent progress on surface modification of Mg-based materials to tailor the degradation rate and biocompatibility for orthopedic applications, and provides a critical analysis of the advantages and limitations of the various surface modification techniques employed.
FRONTIERS IN MATERIALS
(2022)
Article
Materials Science, Multidisciplinary
Mathew Gaius Cherian, Shebeer A. Rahim, V. P. Muhammad Rabeeh, M. A. Joseph, T. Hanas
Summary: Magnesium (Mg) based alloys are potential materials for degradable metallic implants due to their good biocompatibility. This study successfully reduced the degradation rate and enhanced biomineralization through a combination of surface pre-treatment and polymer nanocomposite coating. These findings provide promising material options for the development of degradable metallic implants.
JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE
(2023)
Article
Materials Science, Multidisciplinary
V. P. Muhammad Rabeeh, T. Hanas
Summary: This study investigates the combined effect of gold sputtering and porous microstructure on degradation of iron in physiological environment. The processed sample degrades nearly three times faster than untreated pure iron, and gold-sputtered samples exhibit improved cell compatibility and bioactivity.
MATERIALS TODAY COMMUNICATIONS
(2022)
Article
Chemistry, Medicinal
Merin Joseph, Muhammed Shafeeque Rahman Pathiripparambath, Hanas Tharayil, Ramapurath S. Jayasree, Lakshmi Nair
Summary: Metal-nanocluster-mediated cancer diagnosis and therapy offer a promising approach for effective treatment, by combining multiple therapeutic modalities in a single nanomaterial.
Article
Materials Science, Multidisciplinary
P. P. Muhammed Shafeeque Rahman, Merin Joseph, T. Hanas, Lakshmi Nair
Summary: Point-of-care diagnostics devices are the next generation biosensors for early disease detection, and nano-technology holds greater promise in this field. In this study, an end-to-end aligned gold nanorod is utilized as a sensor for calcium detection in blood serum, and paper-based strips are developed for calcium detection.
Article
Materials Science, Coatings & Films
K. S. Akshay, V. P. Muhammad Rabeeh, Shebeer A. Rahim, K. P. Sijina, G. K. Rajanikant, T. Hanas
Summary: This study investigates the effect of alginate/bioglass composite coating on the biodegradation, bioactivity and biocompatibility of Mg-Ca alloy. The results show that the coated sample has better degradation resistance and bioactivity, and promotes biomineralization and cell adhesion.
SURFACE & COATINGS TECHNOLOGY
(2022)
Article
Materials Science, Biomaterials
V. P. Muhammad Rabeeh, Shebeer A. A. Rahim, Sijina Kinattingara Parambath, G. K. Rajanikant, T. Hanas
Summary: The biocompatibility and biodegradation of iron make it suitable for developing biodegradable metallic implants. Incorporating gold into iron at low concentrations can improve its degradation rate. The Au-incorporated samples showed a significantly faster degradation rate and increased bioactivity compared to pure iron. Integrating nanogold into a Fe matrix promoted the formation of hydroxyapatite and did not cause toxicity to cells.
ACS BIOMATERIALS SCIENCE & ENGINEERING
(2023)
Review
Engineering, Biomedical
V. P. Muhammad Rabeeh, T. Hanas
Summary: This article provides a comprehensive review and analysis of various manufacturing and processing techniques for developing biodegradable iron-based orthopaedic implants. The current status of research in this field is presented, along with a summary of existing works, to help researchers contextualize their own research and identify gaps in the existing scholarship.
PROGRESS IN BIOMATERIALS
(2022)