Journal
CARBOHYDRATE POLYMERS
Volume 222, Issue -, Pages -Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carbpol.2019.114995
Keywords
Nanohybrid; CuO nanoparticles; Bacterial cellulose; Morphology; Bactericidal effect
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Funding
- Iran National Science Foundation (INSF)
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The aim of this research was to fabricate CuO-bacterial cellulose (BC) nanohybrids by two in-situ synthesis methods including sonochemical and precipitation methods. The ex-situ synthesized nanohybrid was also prepared by immersing BC pellicles in commercial CuO dispersion. FT-IR analysis confirmed the formation of real nanohybrid by occurring new interactions between CuO-NPs and BC. XRD results approved no disruption effect of nanohybrid formation on the crystallinity index of BC nanofibers. FE-SEM results indicated the formation of small sized NPs attached to the inner space of BC network at in-situ synthesized nanohybrids. But agglomerated NPs precipitated on the surface of BC layer was observed for ex-situ synthesized sample. In spite of higher loading capacity of ex-situ method, the in-situ synthesized nanohybrids exhibited lower release rate of NPs into the water. The antibacterial activity of ex-situ synthesized nanohybrid against S. aureus and E. coli bacteria was more than both of in-situ synthesized samples.
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